Flame-retardant and insulating epoxy noise-reducing plate and preparation method for same
A technology of insulating rings and plates, applied in chemical instruments and methods, paper/cardboard layered products, lamination, etc., can solve the problems of poor impact strength, collapse, and poor bending strength of laminated boards, and achieve less space occupation. High flame retardancy, easy installation effect
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[0044] At the same time, the present invention also provides a method for preparing a flame-retardant insulating epoxy noise-reducing laminate, said method comprising the following steps:
[0045] (1) Preparation of cured flame retardant epoxy resin glue:
[0046] Add 20-30 parts by weight of dimethylformamide into the container, then add 2.4-3.6 parts by weight of dicyandiamide to dissolve, then add 80-120 parts by weight of flame-retardant epoxy resin, and react at room temperature for 1.5- After 2.5 hours, add 20-30 parts by weight of xylene methylamine, 0.08-0.12 parts by weight of dimethylimidazole, 4-6 parts by weight of acetone and 1.6-2.4 parts by weight of ethanol, and react for 1.5-2.5 hours. Then take a sample test, at 150~170°C, when the polymerization time is in the range of 3.5~4.5min, the preparation of the cured flame retardant epoxy resin glue is completed;
[0047] (2) Preparation of rubber sheet:
[0048] Soak the treated glass cloth in the cured flame-ret...
Embodiment 1
[0058] (1) Preparation of cured flame retardant epoxy resin glue:
[0059] Add 20 parts by weight of dimethylformamide into the container, then add 2.4 parts by weight of dicyandiamide to dissolve, then add 120 parts by weight of flame-retardant epoxy resin, react at room temperature for 1.5 hours, then add 0.08 parts by weight Parts of dimethylimidazole, 4 parts by weight of acetone and 2.4 parts by weight of ethanol, reacted for 1.5 hours, and then sampled and tested. At 150 ° C, when the polymerization time was 3.5 minutes, the cured flame-retardant epoxy resin glue was prepared Complete; wherein, in the cured flame retardant epoxy resin glue solution, the cured flame retardant epoxy resin content is 77.5%.
[0060] (2) Preparation of rubber sheet:
[0061] Soak the treated glass cloth in the cured flame retardant epoxy resin glue prepared in step (1), put the soaked glass cloth into an oven for heating, the steam pressure is 0.7MPa, the temperature is 170°C, and the speed...
Embodiment 2
[0067] (1) Preparation of cured flame retardant epoxy resin glue:
[0068] Add 26.1 parts by weight of dimethylformamide, 3 parts by weight of dicyandiamide, and 100 parts by weight of flame-retardant epoxy resin, react at room temperature for 1.6 hours, then add 0.12 parts by weight of dimethylimidazole, 5.2 parts by weight Parts of acetone and 2 parts by weight of ethanol, reacted for 1.5 hours, at 150 ° C, when the polymerization time was 4.5 minutes, the preparation of the cured flame-retardant epoxy resin glue was completed; wherein, the cured flame-retardant epoxy resin glue In the solution, the cured flame retardant epoxy resin content is 81%.
[0069] (2) Preparation of rubber sheet:
[0070] The steam pressure is 0.65MPa, the temperature is 165°C, and the vehicle speed is 3.4m / min;
[0071] (3), compression molding:
[0072] The pressing pressure is 5.8MPa, the steam pressure is 0.55MPa, the temperature is 155°C, the pressing time is hot pressing for 160 minutes, c...
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