Flame-retardation enhanced epoxy plastic sheet material and its preparation method
A technology of epoxy plastics and plates, applied in the field of polymer material modification and processing, can solve the problems of high cost, high price, unfavorable development of the automobile industry, etc., and achieve the effect of low cost, long life and low cost
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[0038] Example 1
[0039] According to the formula ratio, add 100 parts of epoxy resin, 8 parts of dioctyl phthalate, 5 parts of EPDM rubber, 100 parts of glass fiber, 30 parts of quartz powder, and 10 parts of allyl glycidyl ether into the reactor. , Stir at 70°C for 10 minutes;
[0040] Add 20 parts of chlorinated paraffin and 5 parts of antimony trioxide to the above mixture, heat to 80℃, and stir evenly until no solid particles appear; then add 9 parts of diethylenetriamine-propylene oxide phenyl ether adduct , Stir and mix well;
[0041] Put the prepared liquid under vacuum (vacuum degree is 9.5*10 4 Pa) Stirring, stirring speed 180r / min, degassing for 12 minutes; then put the degassed material in the forming mold for curing, release after 3.5 hours, the mold temperature is 90℃;
[0042] Then the above-mentioned released board is kept at a constant temperature of 55°C for 2 hours. The obtained plates were processed into test strips according to the standard experiment requireme...
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[0043] Example 2
[0044] According to the formula ratio, add 100 parts of epoxy resin, 14 parts of dibutyl phthalate, 8 parts of nitrile rubber, 80 parts of glass fiber, 20 parts of calcium carbonate, and 12 parts of allyl glycidyl ether into the reactor. Stir for 8 minutes at 75°C;
[0045] Add 15 parts of decabromodiphenyl ether and 6 parts of zinc borate to the above mixture, heat to 85°C, and stir evenly until no solid particles appear; then add 5 parts of 2-methylimidazole, stir and mix;
[0046] Put the prepared material liquid under vacuum (vacuum degree is 9.2*10 4 Pa) Stirring, stirring speed 170r / min, degassing for 10 minutes; then put the degassed material in the forming mold for curing, release after 3 hours, the mold temperature is 80℃;
[0047] The above-mentioned released board is kept at a constant temperature of 60°C for 1.5 hours. The obtained plates were processed into test strips according to the standard experiment requirements, and the test properties are liste...
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[0048] Example 3
[0049] According to the formula ratio, add 100 parts of epoxy resin, 6 parts of dinonyl phthalate, 4 parts of EPDM rubber, 120 parts of glass fiber, 60 parts of calcium carbonate, and 8 parts of allyl glycidyl ether into the reactor. , Stir at 80℃ for 8 minutes;
[0050] Add 20 parts of tetrabromobisphenol A and 6 parts of antimony trioxide to the above mixture, heat to 95℃, and stir evenly until no solid particles appear; then add diethylenetriamine-propylene oxide phenyl ether adduct 10 Parts, stir and mix well;
[0051] Put the prepared material liquid under vacuum (vacuum degree is 10.0*10 4 Pa) Stirring, stirring speed 160r / min, degassing for 14 minutes; then put the degassed material in the forming mold for curing, release after 3 hours, the mold temperature is 100℃;
[0052] The above-mentioned released board is kept at a constant temperature of 65°C for 2 hours. The obtained plates were processed into test strips according to the standard experiment requir...
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