Continuous spinning system of poly (p-phenylene terephthalamide)

A technology of poly-p-phenylene terephthalamide and spinning system, which is applied in the direction of spinning solution preparation, filament forming treatment, textile and papermaking, etc. Solving problems such as long time consumption, to achieve the effect of improving production efficiency and finished silk quality, easy reproduction of large-scale industrialization, and easy and smooth material advancement

Inactive Publication Date: 2013-03-06
王泽
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] 1. Due to the dissolution of the reactor, the degassing of the material is an intermittent process, which affects the smooth progress of continuous spinning;
[0007] 2. Due to the low stirring efficiency of the reactor, the mixing and dissolving of materials takes a long time and is difficult to control, the shearing efficiency is low, and the mixing efficiency is poor, which makes it difficult to achieve the desired effect of material dissolution;
[0008] 3. Due to the low stirring efficiency of the defoaming equipment, it takes a long time and the material defoaming efficiency is poor, which seriously affects the subsequent spinning;
[0009] 4. Due to the long time-consuming for dissolution and defoaming, the material is seriously degraded, which affects the product quality;
[0010] 5. Dissolving and defoaming a

Method used

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  • Continuous spinning system of poly (p-phenylene terephthalamide)
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  • Continuous spinning system of poly (p-phenylene terephthalamide)

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0053] Example 1

[0054] Such as figure 1 Shown, a continuous spinning system of poly-p-phenylene terephthalamide, which has spinning dope screw mixing and dissolving machine 24, filter 25, spinning machine 26; spinning dope screw mixing and dissolving machine 24 The material output port is connected to the material input port of the filter 25, and the material output port of the filter 25 is connected to the material input port of the spinning machine 26; the aramid filament spun from the spinning machine 26 is sent to the washing machine 28 through the tractor 27, After being washed with water, it is dried by a dryer 29, and after being oiled by the oiling machine 30, the winding machine 31 is wound into a final product.

[0055] In the system device, the structure of the spinning dope screw mixing and dissolving machine 24 is as Figure 5-11 Shown

[0056] Such as figure 2 As shown, it has a pre-mixing screw extruder 1 and a miscible screw extruder 2; the two ends of the connec...

Example Embodiment

[0075] Example 2:

[0076] A continuous spinning system of poly-p-phenylene terephthalamide. Its structure is basically the same as that of Example 1. The only difference is in the spinning dope screw mixing and dissolving machine 24, such as image 3 As shown, in addition to the feeding section 4, the pre-mixing screw extruder 1 has a mixing section 6. The screw 9 of the feeding section 4 and the mixing section 6 can have different forms, so that the feeding section 4 can quickly transfer the spinning dope. It is fed into the pre-mixing screw extruder, and the mixing section 6 can realize the high-efficiency mixing of the spinning dope; according to the different functions of the feeding section 4 and the mixing section 6, the length ratio between the two can be 1:1~1 :30; The miscible screw extruder 2 has only the miscible section 5, and the exhaust chamber 17 is opened on the miscible section 5.

[0077] The mixing section 6 disperses, mixes PPTA powder and sulfuric acid, and tr...

Example Embodiment

[0078] Example 3:

[0079] A continuous spinning system of poly-p-phenylene terephthalamide. Its structure is basically the same as that of Example 1. The only difference is in the spinning dope screw mixing and dissolving machine 24, such as Figure 4 As shown, the pre-mixing screw extruder 1 has a feeding section 4 and a mixing section 6, and the miscible screw extruder 2 has only a degassing section 7 and a pressure regulating section 8.

[0080] The pressure regulating section 9 adjusts the pressure of the spinning dope coming from the front section, so that the pressure of the material at the screw outlet can better meet the process requirements, and can adjust the pressure of the spinning solution when it enters the spinning link to ensure that the aramid filament is ejected The uniformity of the product can be achieved by single-threaded block 15 or double-threaded block 14 alone or in combination;

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Abstract

The invention provides a continuous spinning system of poly (p-phenylene terephthalamide). The continuous spinning system comprises a spinning raw solution screw rod mixing and dissolving machine, a spinning machine, post-treatment equipment and a winding machine, wherein a spinning raw solution is sufficiently mixed and dissolved in the screw rod mixing and dissolving machine; the mixing is realized by a pre-mixing screw rod extruder; a mixed solution is realized by a mixing screw rod extruder; a connecting piece is arranged between the pre-mixing screw rod extruder and the mixing extruder; a filter is additionally arranged between the mixing screw rod extruder and the spinning machine; a wire bundle is spun by the spinning machine and is wound by the winding machine through the post-treatment equipment to form a final finished product; the post-treatment equipment comprises a traction machine, water washing equipment, drying equipment and an oiling machine; and the equipments are arrayed in a staggered manner. According to the continuous spinning system of the poly (p-phenylene terephthalamide), the defects in the prior art are overcome; the optimized design scheme perfectly fuses three steps including mixing, dissolving and de-foaming; a reasonable post-treatment process is provided and the equipments are arrayed in the staggered manner, so that the production efficiency is high, the quality of the finished product is good and the cost is low; and therefore, the continuous spinning system lays a foundation for large-scale industrialization of an aramid fiber spinning system of China.

Description

technical field [0001] The invention discloses a continuous spinning system of poly-p-phenylene terephthalamide, and more specifically relates to a continuous spinning system capable of industrialized production of poly-p-phenylene terephthalamide, which belongs to Special high-performance fiber production technology field. Background technique [0002] Poly(p-phenylene terephthalamide) has the characteristics and characteristics of high strength, high modulus, high temperature resistance, acid and alkali resistance, organic solvent corrosion resistance, low density, etc., and has appropriate toughness for textile processing. Because poly-p-phenylene terephthalamide has extremely high strength, which is 5 to 6 times that of high-quality steel, its modulus is 2 to 3 times that of steel and glass fiber, its toughness is 2 times that of steel, and its weight is only 1 / 5 of the steel, the silk spun from it has the reputation of "artificial steel wire". "Artificial steel wire" ...

Claims

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Application Information

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IPC IPC(8): D01D1/02D01D1/06D01D1/10D06B23/20
Inventor 张楠张永林张涛许平王泽
Owner 王泽
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