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Raman spectrometer probe and manufacturing method thereof

A technology of a Raman spectrometer and a manufacturing method, which is applied in Raman scattering, material excitation analysis, etc., can solve the problems of slowing down the practical process, difficult pretreatment of optical fiber processing, etc., and achieves the effects of simple structure, low cost, and easy realization.

Active Publication Date: 2015-05-06
FUZHOU PHOTOP QPTICS CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the existing solutions often have problems such as difficult fiber processing or the need for pretreatment, which greatly slows down the practical application of this technology.

Method used

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  • Raman spectrometer probe and manufacturing method thereof
  • Raman spectrometer probe and manufacturing method thereof
  • Raman spectrometer probe and manufacturing method thereof

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Embodiment Construction

[0020] The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.

[0021] A Raman spectrometer probe of the present invention is mainly composed of a multimode optical fiber that transmits excitation light and Raman scattered light at the same time, and its detection end surface is attached with nano-metal microstructure and SiO 2 An aerosol layer; an inert dense layer is attached to the outer surface of the nanometer metal microstructure; the inert dense layer is a chemically inert material. The long-range effect of the strong electromagnetic field enhancement of the nano-metal microstructure is used to enhance the exciting effect of the excitation light on the measured substance, so that the Raman radiation generated by the stimulated substance to be measured is greatly improved, and the intensity of the excitation light is enhanced under the same excitation light intensity. The Raman signal reduces the requ...

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Abstract

The invention discloses a Raman spectrometer probe and a manufacturing method thereof; the structure of the probe comprises a multimode fiber; the detection end face of the multimode fiber is attached with a nanometer metal microstructure and a SiO2 aerosol layer; the external surface of the nanometer metal microstructure is attached with an inert compact layer; the inert compact layer is a chemical inert material. The manufacturing process comprises the following steps: spraying a SiO2 aerosol binder on the detection end face of the multimode fiber, then spraying nanometer metal microsphere particles isolated by the chemical inert material; or coating a nano-scale metal layer on the detection end face of the multimode fiber; etching the surface by lithography technology to obtain a tooth-shaped nanometer metal microstructure, finally coating the SiO2 aerosol layer with a thickness of several nanometers on the surface to form a chemical isolation state. The probe of the invention has higher sensitivity and detection precision, is simple in structure, convenient for manufacturing, and low in cost, needs no pretreatment, and is widely applicable to examination and detection work of various types of trace toxic and harmful substances.

Description

technical field [0001] The invention relates to the field of optical detection instruments, in particular to a Raman spectrometer probe. Background technique [0002] In recent years, melamine, Sudan red and other incidents have exposed huge loopholes in the field of food safety, and the lives and health of the public have been seriously threatened. The detection of low-concentration trace substances has become a research hotspot in food safety testing. Compared with other spectra, Raman spectroscopy can provide rich molecular structure and molecular vibration information, so it has become a powerful tool for material analysis and material identification. However, the Raman scattering cross section is usually in the 10 -30 This is only one thousandth of Rayleigh scattering, and it is very easy to be submerged in the fluorescence background noise, which greatly limits the application of Raman spectroscopy in various fields. [0003] Surface-Enhanced Raman Scattering (SERS) ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N21/65
Inventor 吴砺凌吉武林江铭卢秀爱张扬林磊
Owner FUZHOU PHOTOP QPTICS CO LTD