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Preparation process of leak protection plugging agent along with drilling based on control of dosage of filling agent

A preparation process and filler technology, applied in the field of preparation of anti-leakage and plugging agents while drilling, can solve the problems of reducing drilling efficiency, delaying drilling time, consuming a lot of time, etc., achieving high production efficiency, reducing production costs, and facilitating processing Effect

Inactive Publication Date: 2013-03-27
倪蕊
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0008] The existing plugging methods have their own advantages and disadvantages, but in general they all delay the drilling time more or less and reduce the drilling efficiency. For example, the static plugging method needs to stop drilling. Leakage material changes the performance of the drilling fluid, and it is necessary to readjust the formula of the drilling fluid, etc., which will consume a lot of time, bring great inconvenience to drilling, and lead to large economic losses

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  • Preparation process of leak protection plugging agent along with drilling based on control of dosage of filling agent

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Embodiment

[0030] The invention relates to a preparation process of an anti-leakage plugging agent while drilling based on controlling the dosage of filler, comprising the following steps:

[0031] (a) AM and AMPS are purified for subsequent use;

[0032] (b) Weigh a certain amount of AA and hydrolyze it, and move it into a reaction vessel placed in a super constant temperature water bath;

[0033] (c) adding a certain amount of cross-linking agent;

[0034] (d) add a certain amount of AM and AMPS, adjust the pH value of the reaction system with 10% sodium hydroxide solution;

[0035] (e) After passing inert gas to exhaust oxygen and stirring for about a period of time, add initiator and filler, and the amount of filler is 6%;

[0036] (f) Adjust the temperature to the reaction temperature, and polymerize for a certain period of time to obtain the target product.

[0037] In the step (a), AM and AMPS are purified by ethanol.

[0038] In the step (b), the reaction vessel is a three-ne...

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Abstract

The invention discloses a preparation process of a leak protection plugging agent along with drilling based on the control of dosage of a filling agent. The preparation process comprises the following steps: (a) purifying AM (acrylamide) and AMPS (2-acrylamido-2-methyl propane sulfonic acid) for later use; (b) weighing AA (acrylic acid), hydrolyzing and transferring into a reactor in a super constant-temperature water bath; (c) adding a certain amount of cross-linking agent; (d) adding AM and AMPS solutions, and regulating the pH value of a reaction system; (e) introducing inert gas for deoxygenation, stirring and adding an initiator and the filling agent, wherein the filling agent is of calcium carbonate, and the dosage of the filling agent is 6%; and (f) regulating the temperature to reaction temperature, and performing polymerization reaction for a certain period of time to get a target product. According to the preparation process disclosed by the invention, the leak protection plugging agent along with drilling can be successfully prepared by controlling the type and the dosage of the filling agent in reaction process, the preparation process further has the advantages of high production efficiency, simple production process, simplicity in operation and capability of greatly reducing the production cost, various performances of the produced leak protection plugging agent along with drilling are far better than those of an existing product, and the leak protection plugging agent along with drilling is further conductive to field well leakage treatment.

Description

technical field [0001] The invention relates to a preparation process of an anti-leakage plugging agent while drilling based on controlling the amount of filler added. Background technique [0002] Lost circulation refers to the process of working fluid (including drilling fluid, cement slurry, completion fluid and other working fluids) in the process of various downhole operations such as drilling, cementing, testing or workover in oil and gas exploration and development. It is a kind of downhole complex situation that is lost into the formation under the action of drilling fluid, which is one of the most common and common technical problems in drilling engineering. The reason why it is called an underground complex situation is that most of its occurrences are not caused by human beings and are not transferred by human will. Of course, this statement is not accurate enough. If you encounter a lost channel that can produce lost circulation, but take corresponding effective...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/56C08F220/58C08F220/06C08K3/26C09K8/035C09K8/42
Inventor 倪蕊
Owner 倪蕊