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Method for preparing fructooligosaccharide by taking waste molasses as raw material

A technology of fructooligosaccharides and waste molasses, applied in the direction of fermentation, can solve the problems of prolonging the production cycle of products, harsh working environment, high temperature liquid overflowing and splashing, etc., to achieve good resource protection and comprehensive utilization, speed up adjustment and industrial upgrading , the effect of reducing the amount of labor

Active Publication Date: 2013-05-01
山东星光首创生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are the following problems in this way: (1) Workers directly add powdered activated carbon to the decolorization tank liquid, which will cause a large amount of activated carbon dust to fly, resulting in extremely bad working environment and serious pollution
(2) When the temperature in the decolorization tank rises to 80-100°C, bumping will often occur, causing the high-temperature liquid to overflow and splash, causing personal injury, so there will be certain safety hazards in this process
(3) Activated carbon often floats on the surface of the liquid in large quantities during the contact with the liquid. Even if it is fully stirred, it cannot be fully fused with the sugar solution quickly to achieve the purpose of decolorization as soon as possible. A large amount of waste is usually required during the decolorization process. The stirring time is longer, thus prolonging the product production cycle and causing waste of resources

Method used

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  • Method for preparing fructooligosaccharide by taking waste molasses as raw material
  • Method for preparing fructooligosaccharide by taking waste molasses as raw material

Examples

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Effect test

Embodiment 1

[0018] Mix waste molasses and drinking water into a solution with a concentration of 15% in a certain proportion, and filter it through a nanofiltration membrane. The operation is performed at an average operating temperature of 34~45°C, inlet pressure and outlet pressure of 5~8bar and 4~6bar, respectively. Under certain conditions, when the membrane flux is less than or equal to 2LMH, the feeding is stopped, and the membrane is backwashed with dilute lye. After the dialysate is concentrated with a mass fraction of 52%, add fructosyltransferase, adjust the pH to 5.0, keep warm at 38°C for 10 hours, filter, and use the improved continuous decolorization interchange process to carefully refine the sugar solution. Decolorization and separation process conditions: The pH of the sample solution is 5.0, the sample concentration is 30%, and the sample flow rate is 2. BV / h, that is, 3ml / min. The light transmittance of the column material liquid is ≤85%, and when the conductance of the...

Embodiment 2

[0020] Mix waste molasses and drinking water into a solution with a concentration of 20% in a certain proportion, and filter it through a nanofiltration membrane. The operation is performed at an average operating temperature of 35~45°C, inlet pressure and outlet pressure of 5~8bar and 4~6bar, respectively. Under certain conditions, when the membrane flux is less than or equal to 2LMH, the feeding is stopped, and the membrane is backwashed with dilute lye. The concentrated dialysate solution with a mass fraction of 50% was added with fructosyltransferase to adjust the pH to 5.5, kept at 38°C for 20 hours, filtered, and the improved continuous decolorization interchange process was adopted to carefully refine the sugar solution, decolorization and separation process conditions: The pH of the sample solution is 5.5, the sample concentration is 35%, and the sample flow rate is 2.5 BV / h, that is, 4ml / min. The light transmittance of the material liquid is ≤85%, and when the conduct...

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Abstract

The invention belongs to the technical field of deep processing of agricultural products, and particularly discloses a method for preparing fructooligosaccharide by taking waste molasses as a raw material. The method is characterized in that the method comprises the steps of taking the waste molasses produced during the sucrose refining production course, preparing a waste molasses solution with a mass concentration of 15-20%, dialysing with a 500Da nanofiltration membrane, concentrating a dialysate, adding the dialysate to immobilized transfructosylase directly, adjusting a pH value to be 5-6, saccharifying at 38-42 DEG C for 10-20h, filtering, decolorizing, hybridizing, concentrating, drying, and obtaining the finished solid fructooligosaccharide. According to the method, the waste molasses raw material replaces sucrose for preparing the fructooligosaccharide; the method is abundant in raw material source, simple and easy to operate, low in production cost and reasonable in technological design; the product quality meets a national standard of the fructooligosaccharide; the method is suitable for industrial production; economic benefits can be remarkably increased; and an additional value of a byproduct can be increased.

Description

technical field [0001] The invention belongs to the technical field of deep processing of agricultural products, and in particular relates to a method for preparing fructooligosaccharides from waste molasses. Background technique [0002] my country is an important sugar producing country, and sugar planting occupies an important position in the agricultural economy, ranking fourth after grain, oilseeds, and cotton. Taking Guangxi sugar industry as an example, the sugar mills in the region annually process more than 3 million tons of sugarcane and produce 100,000 tons of waste molasses. Cane molasses contains about 24% to 36% of sucrose, and about 12% to 24% of other sugars; almost all sugars in beet molasses are sucrose, as much as about 47%. In addition, the nitrogen-free extract also contains 3% to 4% soluble colloids, mainly xylose gum, arabic gum and pectin. At present, waste molasses is processed by selling it directly to livestock and poultry farms to feed lives...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C12P19/18
Inventor 曹永兴潘永胜李宁周焕霞张素丽李霞
Owner 山东星光首创生物科技有限公司
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