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Three-primary colours dye and method for detecting two fibers blending ratio of linen to cotton

A technology of cotton and linen fibers and three primary colors, which is used in the preparation of organic dyes, test samples, and color/spectral properties measurement, etc., can solve the problems of long time, large errors, and time-consuming

Inactive Publication Date: 2013-05-01
温演庆 +3
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is time-consuming and has large errors
The dyeing method is based on the principle of dye balance (the amount of adsorption on the fiber is equal to the reduction of dye in the dyeing bath), dyeing a group of linen-cotton blends with a known content of linen-cotton blending, as a standard, using a spectrophotometer Measure the concentration of residual dye solution, calculate the standard curve by linear regression method, and then use the same dyeing process to measure the concentration of residual dye solution to obtain the component content of the sample to be tested. However, the time required for dyeing equilibrium is at least 4 to 5 hours, which takes a long time and the error Generally 5%~8%

Method used

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  • Three-primary colours dye and method for detecting two fibers blending ratio of linen to cotton
  • Three-primary colours dye and method for detecting two fibers blending ratio of linen to cotton
  • Three-primary colours dye and method for detecting two fibers blending ratio of linen to cotton

Examples

Experimental program
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Effect test

Embodiment 1

[0021] Embodiment 1, a kind of trichromatic dyestuff that detects the blending ratio of cotton and linen blend

[0022] The raw material is directly selected as date red GB, the strength is 100%, and the No. 3 Dyestuff Chemical Factory in Tianjin;

[0023] Cationic bright yellow O, strength 100%, Shaoxing Green Chemical Co., Ltd.;

[0024] Disperse blue 2BLN, 100% strength, Zhejiang Runtu Co., Ltd.;

[0025] Penetrant JFC, Jiangsu Haian Petrochemical Plant.

[0026] Weigh 3 g of direct bougainvillea GB, cationic bright yellow O, and disperse blue 2BLN dyes, 9 g in total, and put them into a 1000 mL beaker, add 90 g of penetrant JFC and 90 g of soft water at 40 °C to make the dyes wet and remove them with a glass rod. Stir well, slowly add soft water at room temperature while stirring to fully dissolve and disperse the mixed dye, add soft water at room temperature until the total weight of the liquid is 900 g. The liquid is the three-primary-color dye liquid for detecting th...

Embodiment 2

[0027] Embodiment 2, the method for detecting the fiber blending ratio of cotton and linen blends using three primary color dyeing methods

[0028] Take by weighing 2 g of the three primary color dye solutions of Example 1, put them into a dyeing cup, add soft water to dilute until the total weight is 200 g, stir well to become a dyeing medium; weigh 2 g of the cotton-linen fiber blend to be determined, and immerse in the dyeing medium, Stir with a glass rod for 1 min; put the dyeing cup containing the dyeing medium and the cotton and linen blend to be tested into the HBC-12 swinging room temperature dyeing sample machine (Ronggui Huibao Dyeing and Finishing Machinery Factory, Shunde District, Foshan City), and use 3 The temperature was raised to 95 °C at a rate of °C / min, and the dyeing was maintained at 95 °C for 5 min; after dyeing, the dyed cotton-linen fiber blend was taken out, washed with cold running water for 2 min, and dried in an oven at 40 °C; -Rite 8200 deskto...

Embodiment 3

[0035] Embodiment 3, the method for detecting the fiber blending ratio of cotton / ramie blended fabrics using three primary color dyeing methods

[0036] Desized, scoured and bleached cotton / ramie blends from the market (21 s ×21 s , blending ratio 45 / 55), washed with soft water containing 1g / L penetrant JFC at 50 °C for 30 min, rinsed with cold running water, and dried below 100 °C; weighed 2 g of the treated fabric, according to Example 2 Dyeing, washing and drying described in the "Method of detecting the fiber blending ratio of cotton and linen blends by three primary color dyeing methods"; measuring the dried cotton and linen fibers with an X-Rite 8200 desktop reflection spectrophotometer (X-Rite, USA) Color Tristimulus Values ​​of Blended Fabrics X, Y and Z ;Substitute the chromaticity coordinates x Calculation formula to find the chromaticity coordinates of the dyed matter x = 0.382, substituted into the cotton fiber content linear regression equation C(%) = 2...

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Abstract

The invention relates to a three-primary colours dye and a method for detecting two fibers blending ratio of linen to cotton, and relates to the method for detecting ratio of cotton fiber to linen fiber in a linen-cotton blending fabric, the method comprises the following steps: adding water in a mixture of direct date red GB to cationic bright yellow to disperse blue 2BLN of 1:1:1 according to weight ratio to prepare a three primary colors dye liquid, diluting the three primary colors dye liquid, immersing the linen-cotton fiber blending substrate to be measured and dyeing, using a reflective spectrophotometer to determine the tristimulus values of X, Y and Z of the dried dyed linen-cotton fiber blending substrate; and substituting the tristimulus values in a cotton fiber content linear regression equation to calculate the ratio of the cotton fiber to two fibers of linen and cotton. The three primary colors dye is the dye with high detection precision used for detecting by a dying method. The detection method is simple, the error for detecting two fibers blending ratio of linen to cotton is less than 3%, the speed is rapid, and the detection efficiency is high, and the examination work strength can be greatly reduced.

Description

technical field [0001] The invention relates to a method for identifying the amount of fibers, in particular to a method for detecting the ratio of cotton fibers and hemp fibers in cotton and linen blended fabrics. Background technique [0002] The analysis of fiber blend components usually adopts chemical dissolution analysis method, and there are chemical analysis methods of various fibers in national standards or textile professional standards. This method is based on the difference in chemical properties between the different fiber components in the yarn. The instrument required for this method is simple and the result is reliable. This method only detects a certain kind of hemp fiber or cotton fiber. [0003] But above-mentioned this detection method can not distinguish the hemp fiber or the cotton fiber of the hemp-cotton blended fabric and measure the cotton fiber and the hemp fiber ratio. This is because hemp and cotton belong to cellulose fibers and have similar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/31G01N1/30C09B67/22
Inventor 温演庆朱谱新俞凌云林义
Owner 温演庆
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