Preparation method of negative material of lithium-ion battery for portable game machine
A lithium-ion battery and anode material technology, applied in battery electrodes, circuits, electrical components, etc., can solve the problems of high manufacturing cost, limited large-scale application, low capacity, etc., achieve high graphite cycle performance and improve energy density , the effect of prolonging the service life
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Embodiment 1
[0031] The natural graphite material is crushed by a pulverizer to a particle size below 5μm, and the specific surface area is 100-200m 2 / g, then add potassium borate, the weight of the added additive is 3% of the raw material, mix in the mixer for 4 hours, put the mixed material in the graphitization furnace for purification and graphitization, and continue to feed chlorine gas at 3100 °C, Remove metal impurities in the graphite, put it into a ball mill after cooling, ball mill for 6 hours at a speed of 400 rpm, and pass through a 100-mesh sieve to obtain the processed graphite material.
[0032] Dissolve lead nitrate in toluene to obtain a concentration of 10wt% lead nitrate solution, dissolve epoxy resin in ethylene glycol to obtain a concentration of 15wt% epoxy resin solution, and dissolve ammonia in ethanol to obtain a concentration of 10wt% % solution Ammonia solution.
[0033] The lead nitrate solution and the epoxy resin solution are mixed uniformly according to the...
Embodiment 2
[0042] The natural graphite material is crushed by a pulverizer to a particle size below 5μm, and the specific surface area is 100-200m 2 / g, then add potassium borate, the weight of the added additive is 4% of the raw material, mix in the mixer for 6 hours, put the mixed material in the graphitization furnace for purification and graphitization, and continue to feed chlorine gas at 3300 °C, Remove the metal impurities in the graphite, put it into a ball mill after cooling, ball mill for 4 hours at a speed of 500 rpm, and pass through a 100-mesh sieve to obtain the processed graphite material.
[0043] Dissolve lead nitrate in toluene to obtain a concentration of 25wt% lead nitrate solution, dissolve epoxy resin in ethylene glycol to obtain a concentration of 20wt% epoxy resin solution, and dissolve ammonia in ethanol to obtain a concentration of 15wt% % solution Ammonia solution.
[0044] The lead nitrate solution and the epoxy resin solution are mixed uniformly according to...
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