Real-time fluorescence quantification PCR (Polymerase Chain Reaction) method for detecting ustilago scitaminea
A technology of real-time fluorescence quantification and sugarcane smut, applied in fluorescence/phosphorescence, biochemical equipment and methods, microbial measurement/inspection, etc., can solve the problems of high cost, long cycle, unfavorable detection, judgment and control, etc. Achieve the effect of simple operation, high sensitivity and strong specificity
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Embodiment 1
[0031]Embodiment 1, a kind of real-time fluorescent quantitative PCR method that detects sugarcane smut
[0032] 1. Extraction of Sugarcane Genomic DNA
[0033] Genomic DNA was extracted by the CTAB method, and the specific operations were as follows:
[0034] (1) After wiping the 7 sugarcane samples to be tested with alcohol with a volume concentration of 75%, put them in a mortar, grind them into fine powder with liquid nitrogen, and distribute them in 2 mL centrifuge tubes. The sample volume of each centrifuge tube is 0.2 g;
[0035] (2) Add 900 μL of 2×CTAB extract preheated at 65 °C, shake and mix, incubate in a water bath at 65 °C for 60 min, and mix by inverting every 5 to 10 min;
[0036] (3) After the water bath, take out the centrifuge tube and centrifuge at 12,000 rpm / min for 5 min. Pipette 750 μL of the supernatant into a new 2 mL centrifuge tube, add an equal volume of phenol / chloroform / isoamyl alcohol (volume ratio 25:24:1), shake, 12,000 rpm / min, and...
Embodiment 2
[0066] Embodiment two, the detection of real-time fluorescence quantitative PCR sensitivity
[0067] (1) Comparison test of positive plasmid detection limit
[0068] 100 ng / μL of recombinant b Plasmid DNA was serially diluted 10 times, according to the formula "MW=number of bases×660 dalton / bp, copies / mL=6.02×10 23 ×(concentration g / mL) / (MW g / mol)”, the concentration is 100 ×10 -3 ~100×10 -11 ng / μL diluted sample converted to known copy number is 1.987×10 8 ~1.987×10 1 copies / µL of 8 10-fold gradients b Plasmid DNA template, and then perform real-time fluorescent quantitative PCR and common PCR detection respectively. Among them, the total reaction system of real-time fluorescent quantitative PCR is 25 μL, including 12.5 μL of 2×TaqMan Universal Master Mix, 1 μL of 10 μmol / L quantitative PCR detection primers bEQ-F and bEQ-R, 10 μmol / L Taqman probe 0.2 μL, b Plasmid DNA template 1 μL, ddH 2 Make up to 25 μL with O; the amplification program is: 50 °C, 2 min, 95 °...
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