Method for preparing colored glaze with waste flint glass as raw material
A technology of waste lead-containing glass and colored glaze, which is applied in the field of preparing colored glaze with waste lead-containing glass as raw material, which can solve the problems that the product gloss is not crystal clear, low refractive index, difficult to process, etc., and is easy for large-scale industrial production , good gloss and low softening point
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Embodiment 1
[0017] Step (1). Coarsely crush the CRT screen glass to 1mm, put it into a roller ball mill for fine grinding after coarse crushing, and obtain a finely ground waste lead-containing glass with a particle size of 150 mesh;
[0018] Step (2). Adjust the chemical components of the finely ground waste lead-containing glass, so that the mass percentages of each component in the finely ground waste lead-containing glass are as follows: 55% SiO 2 , 0.1﹪B 2 o 3 , 1﹪ZnO, 3﹪CaO, 2.5﹪BaO, 12﹪Na 2 O, 0.3﹪K 2 O, 20﹪PbO, 6﹪Al 2 o 3 、0.03﹪Er 2 o 3 , 0.07% green colorant; the green colorant is Cr 2 o 3 A mixture with CuO in a mass ratio of 6:1.
[0019] Step (3). Put the finely ground waste lead-containing glass after adjusting the chemical composition into the mixer and mix it evenly, then put it in the tank kiln for high-temperature melting. The melting temperature is 750 °C and the time is controlled for 6 hours. According to the design The shape is artificially formed to obtain ...
Embodiment 2
[0022] Step (1). The CRT cone glass is roughly crushed to 2 mm, and then put into a roller ball mill for fine grinding to obtain a particle size of 200 mesh finely ground waste lead-containing glass;
[0023] Step (2). Adjust the chemical components of the finely ground waste lead-containing glass, so that the mass percentages of each component in the finely ground waste lead-containing glass are as follows: 65% SiO 2 , 0.2﹪B 2 o 3 , 0.2﹪ZnO, 1﹪CaO, 2﹪BaO, 7.49﹪Na 2 O, 0.4﹪K 2 O, 20﹪PbO, 3﹪Al 2 o 3 、0.01﹪Er 2 o 3 , 0.7% dark blue colorant CoO;
[0024] Step (3). Put the finely ground waste lead-containing glass after adjusting the chemical composition into the mixer and mix it evenly, then put it in the pool kiln for high-temperature melting. The melting temperature is 980°C, and the time is controlled for 2 hours. According to the design The shape is artificially formed to obtain the formed product;
[0025] Step (4). Send the formed product into an annealing kiln fo...
Embodiment 3
[0027] Step (1). Crushing the low-melting-point glass sealed by the CRT screen cone to 3 mm, and then putting it into a roller ball mill for fine grinding to obtain finely ground waste lead-containing glass with a particle size of 300 mesh;
[0028] Step (2). Adjust the chemical components of the finely ground waste lead-containing glass, so that the mass percentages of each component in the finely ground waste lead-containing glass are as follows: 50% SiO 2 , 0.3﹪B 2 o 3 , 1﹪CaO, 1.5﹪BaO, 5﹪Na 2 O, 0.1﹪K 2 O, 38﹪PbO, 4﹪Al 2 o 3 , 0.02﹪Er 2 o 3 , 0.08% green colorant; the green colorant is Cr 2 o 3 A mixture with CuO in a mass ratio of 3:1.
[0029] Step (3). Put the finely ground waste lead-containing glass after adjusting the chemical composition into the mixer and mix it evenly, then put it in the pool kiln for high-temperature melting. The melting temperature is 800°C and the time is controlled for 3 hours. According to the design The shape is artificially formed...
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