Surface treatment method of glass flakes for flake resin paint and flake resin paint
A technology for glass flakes and flake resin, which is applied to the surface treatment of glass flakes for flake resin coatings, and the field of flake resin coatings, which can solve problems such as limited effect and so on.
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Embodiment 1
[0039] In this embodiment, a coupling agent is used to pretreat the surface of the glass flakes. The coupling agent is composed of a coupling agent A and a coupling agent B, the coupling agent A is vinyltrialkoxysilane, and the coupling agent B is n-dodecyltrichlorosilane. The specific process is as follows:
[0040] (1) Add coupling agent A to the ethanol solution and mix evenly to form a treatment solution A with a mass percentage concentration of 8%; add coupling agent B to the ethanol solution and mix evenly to form a treatment solution with a mass percentage concentration of 8%. Liquid B;
[0041] (2) Mix perchloric acid and concentrated nitric acid according to the mass ratio of perchloric acid: concentrated nitric acid = 1:1, dilute with deionized water to a concentration of 20% to 60% and stir evenly to form an acid solution. Immerse the glass scales in The acid solution was cleaned and treated for 2 hours, filtered and washed with a large amount of deionized water, ...
Embodiment 2
[0058] In this embodiment, a coupling agent is used to pretreat the surface of the glass flakes. The coupling agent is composed of a coupling agent A and a coupling agent B, the coupling agent A is γ-glycidyl etheroxypropyltrialkoxysilane, and the coupling agent B is octadecyltrichlorosilane. The specific process is as follows:
[0059] (1) Add 1mL of coupling agent A and 1mL of coupling agent B to 120mL of butyl ether solution in turn, mix well to form a mixed treatment solution;
[0060] (2) Mix concentrated sulfuric acid, concentrated nitric acid and water according to the mass ratio of concentrated sulfuric acid: concentrated nitric acid: water = 2:1:2, stir evenly to form an acid solution, and immerse the glass scales in the acid solution for cleaning treatment for 2 hours. After filtering, wash with a large amount of deionized water, then blow dry with nitrogen or put it in a 60-degree oven to dry;
[0061] (3) Slowly pour the mixed treatment solution prepared in step ...
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Abstract
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