Preparation method of polyurethane bandage with functions of promoting blood circulation and removing blood stasis and bandage prepared by method
A technology for promoting blood circulation and removing blood stasis and polyurethane, which is applied in the field of medical and sanitary products, can solve the problems of non-functional polyurethane bandage products, and achieve the effects of promoting early recovery, good plasticity and improving microcirculation.
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[0029] Example 1
[0030] ① Preparation of polyurethane prepolymer
[0031] Add 100 parts of 4,4'-diphenylmethane diisocyanate, 0.5 parts of benzoyl chloride stabilizer and 2.5 parts of organosilicon defoaming agent into a four-neck reactor equipped with a stirrer and a thermometer with high purity nitrogen. After stirring at 45°C for 30 minutes, slowly add 20 parts of polypropylene glycol with a molecular weight of 800-1100, continue to heat and stir for 60 minutes, and then add 35 parts of polypropylene glycol with a molecular weight of 1800-2200 dropwise. After reaction for 2 hours, add the catalyst dimethylethanolamine 3 parts, 5 parts lubricant silicone oil, continue to heat and stir for 15 minutes.
[0032] ②Preparation of chitosan microspheres with drugs for promoting blood circulation and removing blood stasis
[0033] Dissolve 50 parts of chitosan in a 5% acetic acid solution by mass fraction, stir until it is completely dissolved, to obtain the chitosan solution, and then c...
Example Embodiment
[0037] Example 2
[0038] ① Preparation of polyurethane prepolymer
[0039] Add 100 parts of 2,4'-diphenylmethane diisocyanate, 1.8 parts of benzoyl chloride and 3.2 parts of organosilicon defoaming agent into a four-neck reactor equipped with a stirrer and a thermometer with high purity nitrogen. After stirring for 30 minutes at 30°C, slowly add 18 parts of polytetrahydrofuran glycol with a molecular weight of 800-1100, continue heating and stirring for 100 minutes, add 40 parts of polypropylene glycol with a molecular weight of 1800-2200 dropwise, react for 2.5 hours and then add the catalyst triethylene Diamine 1-8 parts, silicone oil lubricant 3-10 parts, continue to heat and stir for 50 minutes.
[0040] ②Preparation of chitosan microspheres with drugs for promoting blood circulation and removing blood stasis
[0041] Dissolve 50 parts of chitosan in a 13% acetic acid solution with a mass fraction of 13%, stir until it is completely dissolved, to obtain the chitosan solution, an...
Example Embodiment
[0044] Example 3
[0045] ① Preparation of polyurethane prepolymer
[0046] Add 100 parts of 4,4'-diphenylmethane diisocyanate, 4.2 parts of propionyl chloride and 3.5 parts of organosilicon defoaming agent into a four-neck reactor equipped with a stirrer and a thermometer into which high-purity nitrogen is introduced. After stirring for 30 minutes at ℃, slowly add 30 parts of polyether triol with a molecular weight of 300-600, continue heating and stirring for 70 minutes, add 10 parts of polytetrahydrofurandiol with a molecular weight of 1800-2200 dropwise, and add organotin catalyst after reaction for 1.5 hours For example, 3 parts of dibutyltin dilaurate and 5 parts of silicone oil lubricant, continue to heat and stir for 45 minutes.
[0047] ②Preparation of chitosan microspheres with drugs for promoting blood circulation and removing blood stasis
[0048] Dissolve 50 parts of chitosan in 15% acetic acid solution, stir until it is completely dissolved, and then centrifuge to coagu...
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