A kind of preparation method of front silver paste
A technology of silver paste and organic carrier, which is applied in the direction of conductive materials dispersed in non-conductive inorganic materials, cable/conductor manufacturing, electrical components, etc., which can solve the problem of affecting the electrical performance of batteries, the difficulty of slurry passing through the screen, and photoelectric efficiency. Reduce problems such as improving performance consistency, facilitating uniform dispersion, and avoiding uneven dispersion
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Embodiment 1
[0027] The present invention is a kind of preparation method of front silver paste, and this method comprises the following steps successively:
[0028] (1) Mix 12% ethyl cellulose, 2% dioctyl phthalate and 86% butyl carbitol by weight percentage, heat to 60~90°C in a water bath, and stir until ethyl cellulose and The dioctyl phthalate is completely dissolved, and the stirring speed is 80-200 rpm to obtain an organic vehicle, and the organic vehicle is kept in a low-viscosity jelly state at 30-40°C for use;
[0029] (2) 93% particle size is 0.1~5 by weight percentage mu m silver powder and 7% particle size is 0.1~3 mu The glass powder of m is added to a ball mill or other mechanical mixer for 5-15 minutes until the solid mixture presents a uniform appearance;
[0030] (3) 1.5kg of the organic carrier obtained in step (1) is added to the rotary mixer, and then 8.5kg of the solid mixture obtained in step (2) is poured into the rotary mixer, and slowly rotated at a speed of 80 ...
Embodiment 2
[0035] The present invention is a kind of preparation method of front silver paste, and this method comprises the following steps successively:
[0036] (1) Mix 12% ethyl cellulose, 2% dioctyl phthalate and 86% butyl carbitol by weight percentage, heat to 60~90°C in a water bath, and stir until ethyl cellulose and The dioctyl phthalate is completely dissolved, and the stirring speed is 80-200 rpm to obtain an organic vehicle, and the organic vehicle is kept in a low-viscosity jelly state at 30-40°C for use;
[0037] (2) 93% particle size is 0.1~5 by weight percentage mu m silver powder and 7% particle size is 0.1~3 mu The glass powder of m is added to a ball mill or other mechanical mixer for 5-15 minutes until the solid mixture has a uniform appearance;
[0038] (3) 1.5kg of the organic carrier obtained in step (1) is added to the rotary mixer, then 0.2g of zinc oxide additive is added to the rotary mixer, stirred at a speed of 200 rpm until the appearance is uniform, and t...
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