A kind of vibrio parahaemolyticus vp nucleic acid constant temperature amplification method
A constant temperature amplification technology for hemolytic vibrio, applied in biochemical equipment and methods, DNA/RNA fragments, and resistance to vector-borne diseases, etc., can solve the problem of inability to distinguish live bacteria from dead bacteria
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Embodiment 1
[0161] Example 1. Design of special primers and probes for detection of Vibrio parahaemolyticus (VP) by real-time fluorescent nucleic acid constant temperature amplification
[0162] In the present invention, the highly conserved segment without secondary structure in the VP toxR gene is selected as the amplified target sequence region (its nucleotide sequence is shown in Sequence 1 in the Sequence Listing), and according to the principle of primer probe design, DNA ATAR, DNAman Software and artificially designed special primers and probe sequences for real-time fluorescent nucleic acid constant temperature amplification detection of Vibrio parahaemolyticus (VP), and obtained the following specific sequences:
[0163] (1) A capture probe (TCO, Target Capture Oligo) that can specifically bind to the target nucleic acid (VP RNA) sequence of Vibrio parahaemolyticus (VP) as shown in Sequence 1 in the sequence listing, the capture probe’s The nucleotide sequence is 5'-aucyuccagucuc...
Embodiment 2
[0167] Example 2 Preparation of a real-time fluorescent nucleic acid constant temperature amplification detection kit for Vibrio parahaemolyticus VP
[0168] Using the special primers and probes provided in Example 1, the real-time fluorescent nucleic acid constant temperature amplification detection kit for Vibrio parahaemolyticus VP of the present invention was obtained. The kit contains capture probe (TCO, Target Capture Oligo), T7 primer, nT7 primer, VP detection probe, internal standard detection probe, internal standard, M-MLV reverse transcriptase and T7 RNA polymerase etc. point.
[0169] Wherein, the capture probe sequence is as SEQ ID NO: 2;
[0170] T7 primer sequence such as SEQ ID NO: 3;
[0171] nT7 primer sequence such as SEQ ID NO: 4;
[0172] EV detection probe sequence such as SEQ ID NO: 5;
[0173] Internal standard detection probe sequence such as SEQ ID NO: 6;
[0174] Internal standard sequence such as SEQ ID NO: 7;
[0175] The capture probe exists...
Embodiment 3
[0208] Example 3 Sensitivity detection of pure bacteria
[0209] With the kit of the present invention (see Example 2 for composition), the detection concentration is 10 2 CFU / mL, 10 3 CFU / mL, 10 4 CFU / mL, 10 5 CFU / mL, 10 6 CFU / mL, 10 7 CFU / mL of Vibrio parahaemolyticus (VP) in food samples, and set up a negative control. The specific method includes the following steps:
[0210] (1) Bacterial culture, counting and dilution
[0211] Take the standard strain of Vibrio parahaemolyticus and streak the alkaline peptone water (APW) plate, culture at 37°C for 12 hours, count by turbidimetry, and dilute with normal saline to quantify to 10 7 CFU / mL, and diluted to 10 times with normal saline 2 CFU / mL.
[0212] (2) Nucleic acid extraction
[0213] 2.1 Add 200 μl of lysate (containing HEPES 35mM, (NH4)2SO4 20mM) and 200μl of sample solution to the sample processing tube (1.5mL centrifuge tube), and use the lysate to lyse the Vibrio parahaemolyticus (VP) in the sample to be...
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