Synergistic insect disinfestation composition containing clothianidin and chlorantraniliprole, and application thereof

A technology of chlorantraniliprole and an insecticidal composition, which is applied in the field of pesticides containing heterocyclic compounds, can solve the problems of narrow insecticidal spectrum, high cost of medication, and easy generation of drug resistance, etc., and achieves inhibition of resistance enhancement, production And the effect of reducing the cost of use and reducing the amount of pesticides used in the field

Inactive Publication Date: 2014-03-12
NANJING HUAZHOU PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] Single-component clothianidin or chlorantraniliprole often has defects in the control of pesticide pests: continuous use is easy to produce r

Method used

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  • Synergistic insect disinfestation composition containing clothianidin and chlorantraniliprole, and application thereof
  • Synergistic insect disinfestation composition containing clothianidin and chlorantraniliprole, and application thereof
  • Synergistic insect disinfestation composition containing clothianidin and chlorantraniliprole, and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Weigh 30 g of clothianidin and chlorantraniliprole, 4 g of calcium dodecylbenzenesulfonate, 3 g of phenethylphenol polyoxyethylene ether, and vegetable oil to 100 g. Put the above raw materials into a mixing tank according to the conventional method for preparing EC and mix them to prepare clothianidin·chlorantraniliprole EC with a main active ingredient of 30% by weight. The specific ratio of clothianidin and chlorantraniliprole is shown in Table 1.

[0024] The rice stem dipping method was used to determine the toxicity of clothianidin, chlorantraniliprole and their compound samples to rice planthoppers. Each treatment was repeated 3 times, and 30 heads were treated at each concentration. 50 Calculate the co-toxicity coefficient according to Sun Yunpei's method:

[0025] Table 1 Toxicity determination and co-toxicity coefficient of clothianidin, chlorantraniliprole and their compound samples to rice planthoppers

[0026]

[0027] The data in the table shows that ...

Embodiment 2

[0029] Weigh clothianidin and chlorantraniliprole and prepare clothianidin-chlorantraniliprole emulsifiable concentrate with a main active ingredient weight percentage of 30% by conventional preparation methods in different proportions. See Table 2 for specific proportions.

[0030] The toxicity of clothianidin, chlorantraniliprole and their compound samples to rice leaf roller was determined by feed poisoning method, each treatment was repeated 3 times, and LC 50 Calculate the co-toxicity coefficient according to Sun Yunpei's method:

[0031] Table 2 Toxicity determination and co-toxicity coefficient of clothianidin, chlorantraniliprole and their compound samples to rice leaf roller

[0032]

[0033] The data in the table shows that clothianidin and chlorantraniliprole have a synergistic effect on the rice leaf roller after being mixed, and the co-toxicity coefficients of the four ratios listed in the table are all far greater than 120. The mixture of chlorantraniliprole...

Embodiment 3

[0035] Weigh 4g of clothianidin, 20g of chlorantraniliprole, 4g of calcium dodecylbenzenesulfonate, 3g of phenethylphenol polyoxyethylene ether, and xylene to 100g, and mix the above raw materials according to the conventional method of preparing emulsifiable concentrate Mix in the kettle to form clothianidin · chlorantraniliprole emulsifiable concentrate whose main active ingredient is 24% by weight.

[0036] The sample prepared in Example 3 was used to carry out the field test of rice planthopper prevention and control in the field. The contrast agent was 15% clothianidin EC and 22% chlorantraniliprole SC. The specific dosage is shown in Table 3, and the water consumption per mu is 30kg. 3 days after the medicine, 7 days, 14 days, 28 days results, the test results are shown in Table 3:

[0037] Table 3 example 3 sample is to the field test result of paddy rice planthopper

[0038]

[0039] It can be seen from Table 3 that Example 3 has an excellent quick-acting effect on...

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Abstract

The present invention discloses a synergistic insect disinfestation composition containing clothianidin and chlorantraniliprole, and an application thereof. The synergistic insect disinfestation composition adopts clothianidin and chlorantraniliprole as main effective components, wherein a weight ratio of the clothianidin to the chlorantraniliprole is 1-100:0.5-80. The synergistic insect disinfestation composition has effects of prevention and control spectrum expanding, synergy and medication cost reduction, can be prepared into an emulsifiable concentrate, wettable powder, a microemulsion, an aqueous emulsion, a suspending agent and water dispersible granules, and is provided for preventing and controlling Lepidoptera, Hemiptera, Hymenoptera, Coleoptera and a plurality of pests.

Description

technical field [0001] The invention belongs to the field of pesticides containing heterocyclic compounds, and in particular relates to an insecticidal composition with clothianidin and chlorantraniliprole as main active ingredients and an application thereof. Background technique [0002] Clothianidin, chemical name: E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine; chemical formula: C 6 h 8 ClN 5 o 2 S; pure product is white crystal, melting point 176.8°C, vapor pressure (20°C) 3.8×10-11Pa, solubility (g / L, 25°C): 0.327 in water (20°C), 2.03 in ethyl acetate, n-heptyl <0.00104 in alkane, 0.0128 in xylene, 1.32 in dichloromethane, 0.938 in octanol, 15.2 in acetone, and 6.26 in methanol. Structural formula: [0003] [0004] Clothianidin acute oral toxicity, male and female rats: LD50>5000mg / kg, acute dermal toxicity: male and female rats: LD50>2000mg / kg, human inhalation toxicity: male and female rats, 6.1mg / L. Clothianidin is a neonicotino...

Claims

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Application Information

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IPC IPC(8): A01N51/00A01N43/56A01P7/04
Inventor 陈文明袁竹青彭永强吴敏沈海峰
Owner NANJING HUAZHOU PHARMA
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