Nano-particle reinforced copper-based composite material and preparation method thereof
A technology of copper-based composite materials and nanoparticles, applied in the direction of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve the problems of poor mechanical properties, high cost, and many processes, and achieve low cost, The effect of long time and many processes
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Embodiment 1
[0025] Put the copper ingot and graphite ingot into the crucible, and put 200g molybdenum on top of the graphite ingot and 5g CaF on top of the copper ingot 2 ;Close the vacuum chamber and start vacuuming; start the rotating device to rotate the substrate at a speed of 6rpm, and turn on the substrate heating device to heat the substrate temperature to stabilize it at 650°C; when the vacuum degree reaches 3×10 -2 At Pa, open the baffle and electron gun, and deposit the isolation layer CaF 2 ;Heat the copper ingot with a beam size of 1.5A, heat the graphite ingot with a beam size of 1.5A, and start to deposit materials. After 50 minutes of deposition, turn off the electron gun, pull up the baffle, turn off the heating device, and turn off the substrate rotation device; when the substrate When the temperature drops below 200°C, turn off the vacuum system, remove the substrate, and separate to obtain a plate with a thickness of 0.26mm and a diameter of 520mm. The composition of t...
Embodiment 2
[0027] Put the copper ingot, molybdenum ingot and anthracene powder into the crucible respectively, and put 5g CaF on top of the copper ingot 2 ;Close the vacuum chamber and start vacuuming; start the rotating device to rotate the substrate at a speed of 15rpm, and turn on the substrate heating device to heat the substrate temperature to stabilize it at 750°C; when the vacuum degree reaches 3×10 -2 At Pa, open the baffle and electron gun, and deposit the isolation layer CaF 2 ;Heat the copper ingot with a beam size of 2.2A, heat the molybdenum ingot with a beam size of 2.6A, heat the anthracene powder with a beam size of 0.6A, and start depositing materials. After 30 minutes of deposition, turn off the electron gun and pull up the baffle. Turn off the heating device, turn off the substrate rotation device; when the substrate temperature drops below 200°C, turn off the vacuum system, remove the substrate, and separate to obtain a plate with a thickness of 0.3mm and a diameter o...
Embodiment 3
[0029] Put the copper ingot, molybdenum ingot and anthracene powder into the crucible respectively, and put 5g ZrO on top of the copper ingot 2 ;Close the vacuum chamber and start vacuuming; start the rotating device to rotate the substrate at a speed of 8rpm, and turn on the substrate heating device to heat the substrate temperature to stabilize it at 650°C; when the vacuum degree reaches 3×10 -2 At Pa, open the baffle and electron gun, and deposit the isolation layer ZrO 2 ;Heat the copper ingot with a beam size of 2.2A, heat the molybdenum ingot with a beam size of 2.0A, heat the anthracene powder with a beam size of 1A, and start to deposit materials. After 40 minutes of deposition, turn off the electron gun, pull up the baffle, and close Heating device, turn off the substrate rotation device; when the temperature of the substrate drops below 200°C, turn off the vacuum system, remove the substrate, and separate to obtain a plate with a thickness of 0.38mm and a diameter of...
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