Deep bleaching method of stevioside
A stevia and deep technology, which is applied in the field of deep decolorization of stevia, can solve the problems of unsatisfactory removal of stevia pigment, affecting the quality and quality of stevia, and it is difficult for the product to achieve pure white, and achieve the best decolorization effect. , low cost, cost saving effect
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Embodiment 1
[0017] Embodiment 1: The deep decolorization method of this stevioside adopts the following specific process steps.
[0018] (1) 100kg of stevia leaves with a stevioside content of 9.39wt% were extracted, flocculated, filtered, resin desalted, and then decolorized with a strong basic anion resin to obtain 450L of decolorized solution, and the 370nm absorbance value of 1% stevioside solution was 0.121; The above steps can adopt the process provided in the publication number CN102649610A "Utilization Method of Wastewater in Stevioside Production".
[0019] (2) Add 2.25L of hypochlorous acid with a concentration of 30wt% to the decolorizing solution, stir evenly, react at 30°C for 4 hours to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no peculiar smell of hypochlorous acid So far, the oxidized liquid is obtained;
[0020] (3) The oxidized liquid flows through the transparent pipeline to pass through the p...
Embodiment 2
[0021] Embodiment 2: The deep decolorization method of this stevioside adopts the following specific process steps.
[0022] (1) 100kg of stevia leaves with a stevioside content of 9.74wt% were extracted, flocculated, filtered, and resin desalted and decolorized to obtain 410L of decolorized solution. The 370nm absorbance value of 1% stevioside solution was 0.094.
[0023] (2) Add 8.2L of hydrogen peroxide with a concentration of 20wt% to the decolorizing solution and stir evenly, react at 30°C for 1 hour to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no peculiar smell of hydrogen peroxide, and the oxidized liquid.
[0024] (2) The oxidized liquid passes through a transparent pipeline irradiated by fluorescent lamps, the temperature of the oxidized liquid is kept at 30-35°C, and the pigment is decomposed by light for 5 hours to decolorize it; it is concentrated and spray-dried to obtain a stevioside pro...
Embodiment 3
[0025] Embodiment 3: The deep decolorization method of this stevioside adopts the following specific process steps.
[0026] (1) 100kg of stevia leaves with a stevioside content of 9.52wt% were extracted, flocculated, filtered, and resin desalted and decolorized to obtain 410L of decolorized solution, and the 370nm absorbance value of 1% stevioside solution was 0.098;
[0027] (2) Add 2.25L of hydrogen peroxide with a concentration of 50wt% to the decolorizing solution and stir evenly, react at 40°C for 3 hours to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no hydrogen peroxide-specific smell, and the oxidized liquid;
[0028] (3) The oxidized liquid passes through a pipeline with a light source, the temperature is kept at 40-45°C, and the center wavelength is 365nm. The ultraviolet light source is irradiated, and the light is irradiated for 1 hour to decompose the pigment to decolorize it; concentrate ...
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