Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Deep bleaching method of stevioside

A stevia and deep technology, which is applied in the field of deep decolorization of stevia, can solve the problems of unsatisfactory removal of stevia pigment, affecting the quality and quality of stevia, and it is difficult for the product to achieve pure white, and achieve the best decolorization effect. , low cost, cost saving effect

Active Publication Date: 2014-04-09
CHENGUANG BIOTECH GRP CO LTD
View PDF3 Cites 10 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the concentration of stevioside is far greater than that of the pigment, if activated carbon is used for adsorption and decolorization, a large amount of stevioside will be adsorbed at the same time; the concentration of 1% stevioside in the solution after decolorization by activated carbon can reach 0.03-0.04 at 370nm; It also took away part of the stevioside ingredients, resulting in a decrease in yield and an increase in cost; moreover, the product is still slightly yellowish and difficult to completely remove, and small activated carbon particles are easily brought into the product and affect the appearance quality of the product
The use of resin decolorization requires a large amount of resin, high investment, and as the use time increases, the decolorization effect will gradually decrease, and the final product is difficult to reach pure white; Basic anion resin and weakly basic anion resin are decolorized twice, but there are still trace pigment residues
[0004] In summary, it is difficult to remove the pigment in stevioside in the existing methods and the effect is not ideal, which seriously affects the quality and quality of stevioside

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Embodiment 1: The deep decolorization method of this stevioside adopts the following specific process steps.

[0018] (1) 100kg of stevia leaves with a stevioside content of 9.39wt% were extracted, flocculated, filtered, resin desalted, and then decolorized with a strong basic anion resin to obtain 450L of decolorized solution, and the 370nm absorbance value of 1% stevioside solution was 0.121; The above steps can adopt the process provided in the publication number CN102649610A "Utilization Method of Wastewater in Stevioside Production".

[0019] (2) Add 2.25L of hypochlorous acid with a concentration of 30wt% to the decolorizing solution, stir evenly, react at 30°C for 4 hours to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no peculiar smell of hypochlorous acid So far, the oxidized liquid is obtained;

[0020] (3) The oxidized liquid flows through the transparent pipeline to pass through the p...

Embodiment 2

[0021] Embodiment 2: The deep decolorization method of this stevioside adopts the following specific process steps.

[0022] (1) 100kg of stevia leaves with a stevioside content of 9.74wt% were extracted, flocculated, filtered, and resin desalted and decolorized to obtain 410L of decolorized solution. The 370nm absorbance value of 1% stevioside solution was 0.094.

[0023] (2) Add 8.2L of hydrogen peroxide with a concentration of 20wt% to the decolorizing solution and stir evenly, react at 30°C for 1 hour to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no peculiar smell of hydrogen peroxide, and the oxidized liquid.

[0024] (2) The oxidized liquid passes through a transparent pipeline irradiated by fluorescent lamps, the temperature of the oxidized liquid is kept at 30-35°C, and the pigment is decomposed by light for 5 hours to decolorize it; it is concentrated and spray-dried to obtain a stevioside pro...

Embodiment 3

[0025] Embodiment 3: The deep decolorization method of this stevioside adopts the following specific process steps.

[0026] (1) 100kg of stevia leaves with a stevioside content of 9.52wt% were extracted, flocculated, filtered, and resin desalted and decolorized to obtain 410L of decolorized solution, and the 370nm absorbance value of 1% stevioside solution was 0.098;

[0027] (2) Add 2.25L of hydrogen peroxide with a concentration of 50wt% to the decolorizing solution and stir evenly, react at 40°C for 3 hours to oxidize the pigment to fade it; pass air into the tank to take out the gas generated by the reaction until the gas has no hydrogen peroxide-specific smell, and the oxidized liquid;

[0028] (3) The oxidized liquid passes through a pipeline with a light source, the temperature is kept at 40-45°C, and the center wavelength is 365nm. The ultraviolet light source is irradiated, and the light is irradiated for 1 hour to decompose the pigment to decolorize it; concentrate ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a deep bleaching method of stevioside. The method comprises the following technological steps: (1) bleaching a stevioside extracting solution or a solution by using resin, so as to obtain a destaining solution; (2) adding an oxidant to the destaining solution, stirring and oxidizing a pigment, so as to obtain oxidized solution; (3) decomposing the pigment from the oxidized pigment in an illumination manner, so as to deeply remove the pigment in the extracting solution or the solution. By adopting the method, the oxidant pigment is added to the yellowish stevioside solution which is bleached by the resin to oxidize, and then the pigment is decomposed in the illumination manner, so that use of activated carbon is avoided, and consumption of the stevioside is reduced. Thus, the cost is saved, and the yield and the product quality are improved. A trace of pigment can be quickly removed by selecting the oxidant and the lighting condition of not generating impurities, so that the color of the product is pure white. Therefore, the deep bleaching method has the characteristics of being simple in technology, significant in effect, high in yield, low in cost, and good in economic benefits, the obtained product is pure white in color, and other impurities are not added.

Description

technical field [0001] The invention relates to a deep processing method of stevioside, in particular to a deep decolorization method of stevioside. Background technique [0002] Stevioside (glycoside) is a new type of natural sweetener extracted from stevia leaves of Compositae herb. It has the characteristics of high sweetness and low calorie. Flavoring agent, known internationally as "the third source of sugar in the world". Widely used in food, beverage and other industries. [0003] During the production process of stevia, the pigment components are removed step by step through flocculation, resin decolorization, activated carbon decolorization and other methods. Since the concentration of stevioside is far greater than that of the pigment, if activated carbon is used for adsorption and decolorization, a large amount of stevioside will be adsorbed at the same time; the concentration of 1% stevioside in the solution after decolorization by activated carbon can reach 0....

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C07H15/256C07H1/06C07H1/08
Inventor 丁红梅牛志平田洪彭静维连运河
Owner CHENGUANG BIOTECH GRP CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products