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Forming copper powder suitable for 3D printing, and manufacturing method and purposes of forming copper powder

A 3D printing, copper powder technology, applied in the direction of improving process efficiency, improving energy efficiency, etc., can solve the problems of low yield of powder, uneven powder melting state, low strength, etc., and achieve high sphericity and particle size. Narrow distribution and high powder yield

Inactive Publication Date: 2014-05-21
KUN SHAN DOTOP METAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the limitation of domestic powder making technology, it is difficult to prepare fine-grained powder, the powder yield is low, and the content of oxygen and other impurities is high. During the 3D printing process, the powder melting state is prone to unevenness, resulting in high oxide inclusion content and denseness in the product. Poor properties, low strength, uneven structure, etc. The main problems of domestic powders are concentrated in product quality and batch stability, including: ① Stability of powder components (inclusion quantity, oxygen content, composition uniformity); ② Stability of powder physical properties (particle size distribution, powder morphology, fluidity, bulk ratio, etc.); ③ Yield problem (low yield of narrow particle size powder), etc.
[0004] At present, most of the materials used in my country's 3D printing rapid prototyping technology need to be imported from abroad, or equipment manufacturers invest a lot of energy and funds in research and development, which is expensive, resulting in increased production costs. Low, localization of 3D printing materials is imperative

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A method for preparing a molded copper powder suitable for 3D printing, said method comprising the steps of:

[0029] (1) Put the TU0 oxygen-free copper into the intermediate frequency induction furnace, heat it to 1250°C under the protection of argon to completely melt the oxygen-free copper, and then blow it into the copper liquid through the embedded gas diffuser at the bottom of the intermediate frequency induction furnace Argon;

[0030] (2) The obtained copper liquid is injected into the leaky crucible under the protection of argon with a pressure of 1KPa. A laminar flow ultrasonic atomizing nozzle is installed under the leaky crucible. When the molten copper flows through the layer through the diversion nozzle When flowing through the ultrasonic atomizing nozzle, it is broken into small droplets by the argon gas preheated at 200 ℃ injected from the nozzle under the atomization pressure of 7MPa, and then the small droplets fall into the atomizing chamber to cool a...

Embodiment 2

[0033] A method for preparing a molded copper powder suitable for 3D printing, said method comprising the steps of:

[0034] (1) Put the TU0 oxygen-free copper into the intermediate frequency induction furnace, heat it to 1400°C under the protection of argon to completely melt the oxygen-free copper, and then blow it into the copper liquid through the embedded gas diffuser at the bottom of the intermediate frequency induction furnace Argon;

[0035] (2) The obtained copper liquid is injected into the leaky crucible under the protection of argon with a pressure of 5KPa, and a laminar flow ultrasonic atomizing nozzle is installed under the leaky crucible. When the molten copper flows through the layer through the diversion nozzle When flowing through the ultrasonic atomizing nozzle, it is broken into small droplets by the argon gas preheated at 400°C injected from the nozzle under the atomization pressure of 10MPa, and then the small droplets fall into the atomizing chamber to c...

Embodiment 3

[0038] A method for preparing a molded copper powder suitable for 3D printing, said method comprising the steps of:

[0039] (1) Put TU0 oxygen-free copper into the intermediate frequency induction furnace, heat it to 1283°C under the protection of argon to completely melt the oxygen-free copper, and then blow it into the copper liquid through the embedded gas diffuser at the bottom of the intermediate frequency induction furnace Argon;

[0040] (2) The obtained copper liquid is injected into the leaky crucible under the protection of argon with a pressure of 2KPa, and a laminar flow ultrasonic atomizing nozzle is installed under the leaky crucible. When the molten copper flows through the layer through the diversion nozzle When flowing through the ultrasonic atomizing nozzle, it is broken into small droplets by the argon gas preheated at 300°C injected from the nozzle under the atomization pressure of 8MPa, and then the small droplets fall into the atomizing chamber to cool a...

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PUM

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Abstract

The invention belongs to the field of materials for 3D printing, and discloses forming copper powder suitable for 3D printing and a manufacturing method of the forming copper powder. The method comprises the steps that TU0 oxygen-free copper is smelted to 1250 DEG C-1400 DEG C by adopting an argon shield furnace, impurities mixed in fused copper liquid are removed by blowing argon at the bottom of the furnace, the copper liquid is completely fused, and temperature evenness is achieved. The fused copper liquid is injected into a tundish crucible by being protected by the argon, the copper liquid flows through a gas atomization nozzle through the tundish crucible and a guide nozzle under stable micropressure, preheated sound-speed argon flow ejected by the gas atomization nozzle washes the surface of the copper liquid to produce shear force and extrusion force, so that the copper liquid deforms, the diameter of the liquid flow becomes smaller and smaller, small liquid drops are formed finally, and then spherical metal powder is manufactured in an atomization chamber in a cooled mode. The 3D printing copper powder manufactured in the method is high in powder obtaining rate, the degree of sphericity is high, the oxygen content is less than 500 ppm, the grain size is less than 10 microns, and distribution is narrow.

Description

technical field [0001] The invention belongs to the field of materials for 3D printing, and relates to a high-performance molding copper powder material for 3D printing, a preparation method and an application thereof. The copper powder material is suitable for laser sintering. Background technique [0002] 3D printing is known as "the engine of the third industrial revolution". Currently, laser sintering and selective laser sintering have brought 3D printing into the "metal age". Some experts pointed out that the core of 3D printing is its subversion of the traditional manufacturing mode. Therefore, in a sense, the most important thing about 3D printing is not mechanical manufacturing, but material research and development. Materials will become the technical commanding heights of 3D printing. On the one hand, the direct manufacturing technology of high-performance metal components and suitable materials can significantly improve the utilization rate of materials, reduce m...

Claims

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Application Information

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IPC IPC(8): B22F9/08B22F3/105B22F3/115
CPCY02P10/25
Inventor 朱胜利
Owner KUN SHAN DOTOP METAL TECH CO LTD
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