A kind of high thermal conductivity plug hole material and preparation method thereof
A high thermal conductivity, plugging technology, applied in the field of electronic materials, to achieve good thermal conductivity, solve local overheating, high thermal conductivity
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Embodiment 1
[0026] A plug hole material, prepared according to the following steps:
[0027] 1) Add the resin diluent isophorone into the plugging resin (specifically, one-component thermosetting epoxy resin), and stir thoroughly for 30 minutes to reduce the viscosity of the plugging resin, among which the plugging resin and resin The mass ratio of diluent is 1:0.02;
[0028] 2) According to the mass ratio of plugging resin and silver-coated copper powder of 1:1.5, weigh the silver-coated copper powder with a particle size of 1-5μm and a silver content of 5-10wt%, and add plasticizer to the silver-coated copper powder Agent dibutyl phthalate and dispersant D-3021 (Rohm and Haas Company), wherein the amount of plasticizer and dispersant are 0.02% and 0.05% of the mass of silver-coated copper powder respectively;
[0029] 3) Transfer the plugging resin diluted in step 1) and the silver-coated copper powder mixed with plasticizer and dispersant in step 2) into a ball mill tank, and add 0.08...
Embodiment 2
[0033] A plug hole material, prepared according to the following steps:
[0034] 1) Add the resin diluent isophorone into the plugging resin (specifically, one-component thermosetting epoxy resin), and stir thoroughly for more than 30 minutes to reduce the viscosity of the plugging resin. The plugging resin and The mass ratio of resin diluent is 1:0.05;
[0035] 2) According to the mass ratio of plugging resin and silver-coated copper powder of 1:2, weigh the silver-coated copper powder with a particle size of 1-5μm and a silver content of 5-10wt%, and add plasticizer to the silver-coated copper powder Agent dibutyl phthalate and dispersant D-3021 (Rohm and Haas Company), wherein the amount of plasticizer and dispersant are 0.05% and 0.08% of the mass of silver-coated copper powder respectively;
[0036] 3) Transfer the plugging resin diluted in step 1) and the silver-coated copper powder mixed with plasticizer and dispersant in step 2) into a ball mill tank, and add 0.1% of ...
Embodiment 3
[0040] A plug hole material, prepared according to the following steps:
[0041] 1) Add the resin diluent isophorone into the plugging resin (specifically, one-component thermosetting epoxy resin), and stir thoroughly for more than 50 minutes to reduce the viscosity of the plugging resin, among which the plugging resin and The mass ratio of resin diluent is 1:0.04;
[0042] 2) According to the mass ratio of plugging resin and silver-coated copper powder of 1:1.7, weigh the silver-coated copper powder with a particle size of 1-5μm and a silver content of 5-10wt%, and add plasticizer to the silver-coated copper powder Agent dibutyl phthalate and dispersant D-3021 (Rohm and Haas Company), wherein, the amount of plasticizer and dispersant are respectively 0.04% and 0.07% of the mass of silver-coated copper powder;
[0043] 3) Transfer the plugging resin diluted in step 1) and the silver-coated copper powder mixed with plasticizer and dispersant in step 2) into a ball mill tank, a...
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