Preparation method of salt-tolerant super absorbent polymer (SAP)
A water-absorbent resin and salt-resistant technology, applied in the field of water-absorbent resin preparation, can solve the problems of poor temperature resistance, high price, single raw material, etc.
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[0011] DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention is further described and illustrated below through specific embodiments:
[0012] Weigh 3g of maleic acid, prepare a solution, add 25% NaOH solution to adjust the neutralization degree (N) of maleic acid to 80%; accurately weigh 5g of acrylamide, 2g of 2-acrylamido-2-methylpropane Put the sulfonic acid in a 250mL three-necked flask, add distilled water and stir to make it evenly dispersed; pour the maleic acid solution into the three-necked flask, add a certain amount of distilled water to make w(MA+AM+AMPS)=20% (based on the quality of the system ); then add 0.1% mass fraction of cross-linking agent N,N'-methylenebisacryloyl solution, heat up to 50°C; stir at a speed of less than or equal to 100rpm for 10 minutes, then dropwise add 0.2% mass fraction of initiator over Ammonium sulfate-sodium bisulfite solution, continue to stir until uniformly mixed; nitrogen gas is introduced to maintain a constan...
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