Sputtering target for magnetic recording medium, and process for producing same
A technology for magnetic recording medium and manufacturing method, which is applied in the direction of sputtering coating, sputtering coating, disc carrier manufacturing, etc., can solve the problems of inability to increase the leakage magnetic flux density, inability to introduce strain, etc., to prevent or Suppresses the generation of nodules and granules, improves the quality, and improves the manufacturing yield
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Embodiment 1
[0073] A Co-Cr-Pt-B alloy raw material containing Cr: 15 at%, Pt: 14.5 at%, B: 8 at%, the balance being Co and unavoidable impurities was subjected to high-frequency (vacuum) melting. The smelted raw material was cast on a copper flat plate using a mold made of cobalt at a temperature from the melting point to the melting point+100° C. to obtain an ingot of 180×300×33 t.
[0074] Next, this ingot was subjected to primary rolling at a total rolling reduction rate of 62%. At this time, the annealing temperature during hot rolling was set to 1090°C. Then, the obtained rolled material was subjected to secondary rolling at a total rolling reduction rate of 5.0%. Then, this is machined and finished into a target.
[0075] The surface parallel to the sputtering surface of the target was observed with an electron microscope FE-EPMA (model: JXA-8500F) manufactured by JEOL, in arbitrary 10 fields (areas) of 190 μm×240 μm. Results The average particle area of the B-rich phase was 77...
Embodiment 2
[0080] As shown in Table 1, the composition ratio was adjusted to Co-15Cr-17.5Pt-8B, and the target was produced by the same production method as in Example 1. At this time, the ingot size after casting was 180×300×36t. In addition, the annealing temperature was set to 1090° C., the total rolling ratio of the primary rolling was set to 86%, and the total rolling ratio of the secondary rolling was set to 4.2%.
[0081] Analyze the target according to the same method as in Example 1, and the results are shown in Table 1. The average particle area of the B-rich phase is 44.6 μm 2 , the rupture number of B-rich phase is 1500 / mm 2 . In addition, the maximum magnetic permeability with respect to the horizontal direction of the sputtering surface was 8.3.
Embodiment 3
[0083] As shown in Table 1, the composition ratio was adjusted to Co-15Cr-11Pt-12B, and the target was produced by the same production method as in Example 1. At this time, the annealing temperature was set to 1100° C., the total rolling ratio of the primary rolling was set to 73%, and the total rolling ratio of the secondary rolling was set to 3.6%.
[0084] Analyze the target according to the same method as in Example 1, and the results are shown in Table 1. The average particle area of the B-rich phase is 84.9 μm 2 , the rupture number of B-rich phase is 2000 / mm 2 . In addition, the maximum magnetic permeability with respect to the horizontal direction of the sputtering surface was 11.
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