Organosilicone defoamer and preparation method thereof
A technology of silicone defoamer and defoamer, which is applied in the direction of foam dispersion/prevention, can solve the problems of product quality and production capacity decline, affect the normal production, reduce the effective load of equipment, etc., and achieve a wide range of applications , easy operation, excellent stability and dispersibility
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Embodiment 1
[0013] The raw material weight percent composition of described organosilicon defoamer: high boiling silicone oil 15%, dimethyl silicone oil (viscosity 600mPa·s) 14%, fumed white carbon black 3%, composite emulsifier (composite by Span80 and Tween80, m Span80 :m Tween80 =1:1.14) 20%, deionized water 46%, thickener (polyvinyl alcohol) 2%. The preparation process is:
[0014] (1) Put dimethyl silicone oil and fumed silica into the reaction kettle according to the above ratio, raise the temperature to 150°C, and stir for 5-8 hours to prepare silicone paste;
[0015] (2) Add high-boiling silicone oil into the silicone paste, then add emulsifier, mix evenly, heat up to 40°C and stir for 30 minutes, add deionized water and polyvinyl alcohol, mix and stir for 4 hours, then cool and pack.
Embodiment 2
[0017] The raw material weight percent composition of described organosilicon defoamer: high boiling silicone oil 20%, dimethyl silicone oil (viscosity 510mPa·s) 20%, fumed white carbon black 3%, composite emulsifier (compounded by Span80 and Tween80, m Span80 :m Tween80 =1:1) 15%, deionized water 40%, thickener (polyvinyl alcohol) 2%. The preparation process is:
[0018] (1) Put dimethyl silicone oil and fumed silica into the reaction kettle according to the above ratio, raise the temperature to 150°C, and stir for 5-8 hours to prepare silicone paste;
[0019] (2) Add high-boiling silicone oil to the silicone paste, then add emulsifier, mix well, heat up to 40°C and stir for 30 minutes, add deionized water and polyvinyl alcohol, mix and stir for 2 hours, then cool and pack.
Embodiment 3
[0021] The raw material weight percent composition of described organosilicon defoamer: high boiling silicone oil 15%, simethicone oil (viscosity 728mPa·s) 22%, fumed white carbon black 3%, composite emulsifier (composite by Span80 and Tween80, m Span80 :m Tween80 =1:1) 8%, deionized water 49%, thickener (polyvinyl alcohol) 3%. The preparation process is:
[0022] (1) Put dimethyl silicone oil and fumed silica into the reaction kettle according to the above ratio, raise the temperature to 150°C, and stir for 5-8 hours to prepare silicone paste;
[0023] (2) Add high-boiling silicone oil to the silicone paste, then add emulsifier, mix well, heat up to 40°C and stir for 30 minutes, add deionized water and polyvinyl alcohol, mix and stir for 3 hours, then cool and pack.
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