Magnetron sputtering cluster ion source used for flight time mass spectrum
A technology of time-of-flight mass spectrometry and magnetron sputtering, which is applied in the field of ion sources, can solve the problems that the same type of magnetron sputtering components cannot be accurately analyzed, and the size of metal clusters is small, so as to achieve accurate composition analysis and reduce loss.
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[0018] The target material is a silver target with a diameter of 50.8 mm and a thickness of 4 mm. The magnetron sputtering head is supplied with cooling water, 30 ml of argon gas per minute, and 120 ml of helium gas per minute. Turn on the DC power supply of magnetron sputtering, the voltage is 300V, the current is 0.2A, the generated ions directly enter the time-of-flight mass spectrometer, the acquisition frequency is 10000Hz, and the accumulation is 500 seconds to obtain Ag n + and Ag n o + (n=1-34) time-of-flight mass spectrometry (eg image 3 shown), indicating that time-of-flight mass spectrometry can be used to accurately analyze Ag 1 + and Ag 1 o + to Ag 12 + and Ag 12 o + Isotopic peaks with an accuracy of 1 Dalton (Da). Optimize the conditions of the magnetron sputtering ion source to produce large-sized silver clusters and silver oxide clusters. The acquisition conditions are the same as above, such as Figure 4 As shown, the measurement range of time-of...
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