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Preparation method of industrial antitoxin efficient impregnated carbon

An impregnated carbon, high-efficiency technology, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve problems such as inability to meet protection requirements, achieve timely and effective purification efficiency, good versatility, and universality strong effect

Inactive Publication Date: 2015-02-04
SHANXI XINHUA CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although there are various types of impregnated carbons on the market, such as NH3 impregnated carbons, H2S, SO2 impregnated carbons, NOx protective materials, HCN, CHCL protective materials, etc., but in terms of protection objects, these impregnated carbons are currently Carbon can only meet the protection of a certain kind or a certain type of toxic and harmful substances. When it is too late to figure out the types of toxic and harmful gases and the types of toxic and harmful gases are complicated, the above impregnated carbon cannot meet the protection requirements.

Method used

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  • Preparation method of industrial antitoxin efficient impregnated carbon

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] An industrial anti-toxic high-efficiency impregnated carbon, using coconut shell crushed activated carbon as the carrier skeleton material, loaded with 15% (weight) of Cu, 2% (weight) of Mo, 3% (weight) of Zn, 4% (weight) ) CO 3 2- , 10 wt% SO 4 2- .

[0024] Wherein, the weight of the carrier material activated carbon is 100%, such as activated carbon 100g, copper 15g, molybdenum 2g, zinc 3g, carbonate ion 4g, sulfate ion 10g; then active component basic copper carbonate 25.5g, molybdic acid Ammonium 4g, basic zinc carbonate 5.4g, ammonium carbonate 6.4g, ammonium sulfate 14g.

[0025] The preparation method of above-mentioned efficient impregnated carbon is as follows:

[0026] (1) Mixed solution configuration: Add the impregnating agent containing the above active components into the calculated mixed solvent of ammonia water and distilled water (the ratio of ammonia water to distilled water is 20:1; use the same amount of impregnation method, and those skilled i...

Embodiment 2

[0030] An industrial anti-virus high-efficiency impregnated carbon, using coconut shell crushed activated carbon as the carrier skeleton material, loaded with 18% (weight) of Cu, 4% (weight) of Mo, 1.5% (weight) of Zn, 2% (weight) ) CO 3 2- , 8 wt% SO 4 2- .

[0031] Wherein, the weight of the carrier material activated carbon is 100%, such as activated carbon 100g, copper 18g, molybdenum 4g, zinc 1.5g, carbonate ion 2g, sulfate ion 8g; then the active component basic copper carbonate 30.6g, molybdenum Ammonium acid 8g, basic zinc carbonate 2.7g, ammonium carbonate 3.2g, ammonium sulfate 11.2g.

[0032] The preparation method of above-mentioned efficient impregnated carbon is as follows:

[0033](1) Mixed solution configuration: Add the impregnating agent containing the above active components into the calculated mixed solvent of ammonia water and distilled water (the ratio of ammonia water and distilled water is 20:1; use the same amount of impregnation method, the amoun...

Embodiment 3

[0037] An industrial anti-toxic high-efficiency impregnated carbon, using coconut shell crushed activated carbon as the carrier skeleton material, loaded with 20% (weight) of Cu, 5% (weight) of Mo, 0.5% (weight) of Zn, 5% (weight) ) CO 3 2- , 5 wt% SO 4 2- .

[0038] Wherein, the weight of the carrier material activated carbon is 100%, such as activated carbon 100g, copper 20g, molybdenum 5g, zinc 0.5g, carbonate ion 5g, sulfate ion 5g; then the active component basic copper carbonate 34g, molybdenum acid Ammonium 10g, basic zinc carbonate 0.9g, ammonium carbonate 8g, ammonium sulfate 7g.

[0039] The preparation method of above-mentioned efficient impregnated carbon is as follows:

[0040] (1) Mixed solution configuration: Add the impregnating agent containing the above active components into the calculated mixed solvent of ammonia water and distilled water (the ratio of ammonia water and distilled water is 20:1; use the same amount of impregnation method, the amount use...

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Abstract

The invention belongs to the technical field of impregnated carbon, and particularly relates to efficient impregnated carbon capable of effectively purifying multiple industrial toxic and harmful gases in a complex environment. The efficient impregnated carbon adopts broken coconut shell activated carbon as carrier framework material, and the carrier framework material is loaded with 13wt%-20wt% of Cu, 2wt%-6wt% of Mo, 0.1wt%-3wt% of Zn, 0-7wt% of CO3<2-> and 5wt%-10wt% of SO4<2->. The impregnated carbon provided by the invention is high in generality, good in universality and wide in protection spectrum, can meet the purification demand and the protection demand of the complex environment, is capable of effectively purifying gases in time especially under the condition that the types of the toxic and harmful gases can not be figured out in time and the varieties of the toxic and harmful gases are complicated, and is in accordance with the demand of market development.

Description

technical field [0001] The invention belongs to the technical field of impregnated carbon, and provides a method for preparing high-efficiency impregnated carbon that can be used in complex environments to effectively purify various industrial toxic and harmful gases. Background technique [0002] Activated carbon and its impregnated carbon are the core poison filter materials of chemical defense equipment (including individual combat protective equipment and cluster protective equipment) that were gradually developed and widely used after the two world wars. With the development of chemical warfare, the research on military poisons in various countries is increasing and deepening, and the development of impregnated carbon is also changing with each passing day, from the initial activated carbon, single-component loading (A-type activated carbon catalyst) to multi-component loading ( AS type, ASC type, ASC-T type and ASZM-T type activated carbon catalyst, etc.), from the ini...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J27/232
Inventor 赵婷金彦任赵存丹齐嘉豪王德周安丽花郭军军裴佩周闯张金凤黄英范斌杰
Owner SHANXI XINHUA CHEM
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