The utility model discloses a purification device of 2, 3, 5, 6-tetrachloropyridine. Comprising a crude product
storage tank, a first-stage
storage tank, a liquid alkali
storage tank, a first-stage rectifying
tower, a neutralizing tank, an extraction layering tank, a second-stage rectifying
tower, a third-stage rectifying
tower, a waste storage tank, a triple-effect
evaporation device, a crude salt storage tank, a low-boiling-point mixture
receiver, a finished product storage tank, a
reboiler, a first condenser, a second condenser and a third condenser. The crude product storage tank is connected with an inlet of the first-stage storage tank through a pipeline, the side surface of the first-stage storage tank is connected with an inlet of the first-stage rectifying tower through a pipeline, and a bottom outlet of the first-stage storage tank is connected with an inlet of the
reboiler through a pipeline; according to the utility model, multiple functions of mixing, extracting and rectifying are combined, high-purity 2, 3, 5, 6-tetrachloropyridine can be produced so as to meet the purity requirement of downstream products on 2, 3, 5, 6-tetrachloropyridine, and meanwhile, high-concentration salt-containing
wastewater generated in the extraction process is subjected to triple-effect
evaporation to obtain industrial salt for use.