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Membrane concentration process for preparing xylitol from viscose production pressed liquor

The technology of viscose fiber and pressing liquid is applied in the field of preparation of xylitol, which can solve the problem of high cost and achieve the effects of low cost, cost reduction and high process operation efficiency.

Inactive Publication Date: 2015-02-18
YIBIN GRACE GROUP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The patent uses industrial ethanol to extract hemicellulose, which is costly

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] A kind of membrane concentration process that viscose fiber is produced and squeezed liquid is prepared xylitol, concrete process steps are as follows:

[0050] A. Membrane concentration

[0051] The squeezed liquid produced by viscose fiber is pre-filtered to remove large particles of impurities, and the permeate is concentrated twice through the nanofiltration membrane cycle, and the last concentrated liquid is diluted with water and then sent to ceramic membrane for filtration, and the obtained concentrated liquid is squeezed soda The concentrated solution of the liquid; the nanofiltration membrane is concentrated twice in circulation, and before each filtration, the feed liquid enters the nanofiltration membrane after being diluted with water.

[0052] B. Extract semi-fiber

[0053] Add acid to neutralize the concentrated solution of the squeezed lye to obtain a semi-fiber liquid.

[0054] C. Enzymolysis

[0055] Add complex enzymes to the semi-fiber liquid, enzy...

Embodiment 2

[0061] A kind of membrane concentration process that viscose fiber is produced and squeezed liquid is prepared xylitol, concrete process steps are as follows:

[0062] A. Membrane concentration

[0063] The squeezed liquid produced by viscose fiber is pre-filtered to remove large particles of impurities, and the permeate is concentrated through the nanofiltration membrane for 3 times, and the last concentrated liquid is diluted with water and then sent to the ceramic membrane for filtration, and the obtained concentrated liquid is squeezed soda The concentrated solution of the liquid; the nanofiltration membrane is concentrated 3 times in circulation, and before each filtration, the feed liquid enters the nanofiltration membrane after being diluted with water.

[0064] B. Extract semi-fiber

[0065] Add acid to neutralize the concentrated solution of the squeezed lye to obtain a semi-fiber liquid.

[0066] C. Enzymolysis

[0067] Add complex enzymes to the semi-fiber liquid...

Embodiment 3

[0073] A kind of membrane concentration process that viscose fiber is produced and squeezed liquid is prepared xylitol, concrete process steps are as follows:

[0074] A. Membrane concentration

[0075] The squeezed liquid produced by viscose fiber is pre-filtered to remove large particles of impurities, and the permeate is concentrated 4 times through the nanofiltration membrane cycle, and the last concentrated liquid is diluted with water and then sent to ceramic membrane for filtration, and the obtained concentrated liquid is squeezed soda The concentrate of the liquid; the nanofiltration membrane is concentrated 4 times in circulation, and before each filtration, the feed liquid enters the nanofiltration membrane after being diluted with water.

[0076] B. Extract semi-fiber

[0077] Add acid to neutralize the concentrated solution of the squeezed lye to obtain a semi-fiber liquid.

[0078] C. Enzymolysis

[0079] Add complex enzymes to the semi-fiber liquid, enzymatic ...

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Abstract

The invention provides a membrane concentration process for pressing xylitol from viscose pressed liquor. The membrane concentration process comprises the following specific process steps: A, performing membrane concentration, wherein the viscose production pressed liquor is firstly prefiltered to remove large-particle impurities, penetrated liquor is circularly concentrated 2-4 times by virtue of a nanofiltration membrane, concentrated liquor obtained at the last time is diluted by being added with water and then fed into a ceramic membrane for being filtered, and the obtained concentrated liquor is the concentrated pressed alkali liquor; the feed liquor is diluted by being added with water and then enters the nanofiltration membrane before the penetrated liquor is filtered when the penetrated liquor is circularly condensed 2-4 times by virtue of the nanofiltration membrane; B, extracting hemicellulose to neutralize the concentrated pressed alkali liquor by adding acid to obtain hemicellulose liquid; C, performing enzymolysis, wherein compound enzyme is added into the hemicellulose liquid to generate enzymatic hydrolysis to obtain enzymatic hydrolysate; D, fermenting, wherein the enzymatic hydrolysate is fermented for 0.5-2 hours at 50-60 DEG C under the action of candida mycoderma bacteria; and E, purifying, wherein the fermented liquor is ultra-filtered to remove impurities, and the penetrated liquor is desalinized by virtue of the nanofiltration membrane, the obtained concentrated liquor is purified liquor of xylitol, and the xylitol is obtained by virtue of ion exchange, active carbon treatment, concentration and crystallization and separation.

Description

technical field [0001] The invention relates to the field of preparation of xylitol, in particular to a process for preparing xylitol by using pressed lye produced by viscose fiber as a raw material. Background technique [0002] The sweetness of xylitol is equivalent to sucrose, and the heat is equivalent to glucose. Xylitol can adjust the abnormality of sugar metabolism and is a nutritional and therapeutic agent for diabetics. Xylitol has a strong anti-ketone body effect and can be used to rescue patients with ketone bodies. Xylitol can slow down the production of fatty acids in plasma, but it will not increase blood sugar. It is also a liver-protecting drug for patients with hepatitis. Xylitol has good thermal stability and does not produce chemical reactions when heated together with amino acids. It can be formulated with amino acids in various preparations as nutraceuticals. As a food, xylitol also has a special anti-caries function. However, xylitol is one of the mo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C12P7/18B01D61/58C12R1/72
CPCC12P7/18B01D61/58
Inventor 邓传东冯涛孙毅唐孝兵莫世清周林罗红梅
Owner YIBIN GRACE GROUP CO LTD
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