Dual-function electric conduction silver paste for touch screen and preparation method and application thereof
A conductive silver paste and touch screen technology, which is applied in the manufacture of cables/conductors, conductive materials dispersed in non-conductive inorganic materials, circuits, etc., can solve the problems of cumbersome procedures, low utilization of materials and man-hours, and reduced production costs. Achieve the effects of high adhesion strength, complete silver electrode wire functionality, and high yield
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[0035] The preparation method of the conductive paste of the embodiment of the present invention comprises the following steps:
[0036] (1) preparing an organic carrier, further comprising the steps of:
[0037] (1-1) The molecular weight is lower than 600 terminal hydroxyl linear alcohol polyester as the monomer of the structural resin, in N 2 Heating and stirring under air protection, react polyester and TDI at 40-60°C for 1-1.5 hours, add organic solvent, after the prepolymer is dissolved, add chain extender R(OH)x dropwise, and react The temperature rises to 70-90°C, and when the viscosity of the system reaches the required value, the reaction is stopped with alcohol to obtain a modified polyurethane with a number-average molecular weight of 8,000-12,000;
[0038] (1-2) Modified polyurethane, latent curing agent and diluent are dispersed by a high-speed disperser to prepare an organic vehicle.
[0039] (2) preparing a dual-functional conductive silver paste for a touch ...
Embodiment 1
[0042] in N 2 Heating and stirring under the protection of air, react the hydroxy-terminated neopentyl alcohol polyester and TDI at 40°C for 1.25 hours, add tetrahydrofuran / tert-butyl methyl ether (V:V=3:1), after the prepolymer is dissolved, drop Add chain extender pentaerythyl glycol, and raise the reaction temperature to 80°C, stop the reaction with alcohol when the viscosity of the system reaches the required value, and obtain a modified polyurethane with a number average molecular weight of 8000;
[0043] The latent curing agent blocked polyisocyanate (DesmodurBL) is added to the modified polyurethane with a molecular weight of 8000 at an active hydroxyl equivalent ratio of 1:1, and dibutyltin dilaurate with a curing agent of 1wt‰, and diluent DBE / 150# (V : V=7:3), the organic vehicle was prepared after being dispersed by a high-speed disperser.
[0044] Weigh raw materials according to the following mass percentage: 73% bulk density is 2.0g / cm 3 , The tap density is 4....
Embodiment 2
[0047] in N 2 Heat and stir under the protection of air, react the hydroxyl-terminated neopentyl alcohol polyester and TDI at 50°C for 1 hour, add tetrahydrofuran / dimethylformamide (V:V=2:1), after the prepolymer is dissolved, Add the chain extender trimethylolpropane dropwise, raise the reaction temperature to 70°C, stop the reaction with alcohol when the viscosity of the system reaches the required value, and obtain a modified polyurethane with a number average molecular weight of 10,000;
[0048] The latent curing agent blocked polyisocyanate (DesmodurBL) is added to the modified polyurethane with a molecular weight of 10000 at an active hydroxyl equivalent ratio of 1.4:1, and dibutyltin dilaurate with a curing agent of 1wt‰, and diluent DBE / 70# (V : V=7:3), the organic vehicle was prepared after being dispersed by a high-speed disperser.
[0049] Weigh raw materials according to the following mass percentage: 60% bulk density is 1.1g / cm 3 , The tap density is 3.2g / cm 3 ...
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