Electronic cigarette smoke solution prepared through dark green tea leaf extract
A technology of tea extract and e-cigarette liquid, which is applied in the field of e-cigarettes, can solve problems such as poor taste and insufficient aroma, achieve rich aroma, solve the problem of insufficient aroma and taste, and coordinate aroma
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Embodiment 1
[0051] Preparation of tobacco extract: take Luzhou-flavor flue-cured tobacco leaf samples, dry them in an oven at 40° C. for 3 hours, cool to room temperature, and crush them to 40-100 meshes. Weigh 100g of tobacco powder into a 1L Erlenmeyer flask, add 300mL of deionized water, conduct ultrasonic extraction at 50±5°C for 4 hours, then let it settle for 4 hours, filter it with a sand core funnel to obtain the filtrate, and depressurize at 70±10°C Concentrate to 3mL by rotary evaporation to obtain tobacco extract.
[0052] The supercritical preparation method of black tea leaf extract: Weigh 100g of Yunnan Puer tea, grind it into 20-30 mesh powder through a pulverizer, put it into a 1L extraction kettle, control the extraction pressure to 25MPa, and the extraction temperature to 50°C. Regulation of supercritical CO 2 The flow rate is 25L / h, and the extraction time is 3h. After extraction, the supercritical fluid dissolved with the extract is decompressed through the throttle ...
Embodiment 2
[0057] Preparation of tobacco extract: take a Burley tobacco leaf sample, dry it in an oven at 40° C. for 3 hours, cool it to room temperature, and crush it to 40-100 mesh. Weigh 100g of tobacco powder into a 1L Erlenmeyer flask, add 300mL of deionized water, ultrasonically extract at 50±5°C for 4 hours, then let it settle for 4 hours, filter with a sand core funnel to obtain the filtrate, and decompress at 70±10°C Concentrate to 3mL by rotary evaporation to obtain tobacco extract.
[0058] The supercritical preparation method of black tea leaf extract: Weigh 100g of Hunan Fuzhuan brick tea, grind it into 45-55 mesh powder through a pulverizer, put it into a 1L extraction kettle, control the extraction pressure to 40MPa, and the extraction temperature to 35°C. Regulation of supercritical CO 2 The flow rate is 35L / h, and the extraction time is 5h. After extraction, the supercritical fluid dissolved with the extract is decompressed through the throttle valve and enters the sep...
Embodiment 3
[0063] Tobacco extract preparation: take a sample of cut tobacco of Nicotiana japonica, and extract, the extraction method is the same as that in Example 1.
[0064] The supercritical preparation method of black tea leaf extract: weigh 100g of Hubei green brick tea, grind it into 10-20 mesh powder through a pulverizer, put it into a 1L extraction kettle, control the extraction pressure to 50MPa, and the extraction temperature to 55°C. Supercritical CO 2 The flow rate is 20L / h, and the extraction time is 7h. After extraction, the supercritical fluid dissolved with the extract is decompressed through the throttle valve and enters the separation kettle to become a gas. The extract is precipitated in the separation kettle and collected in the receiving bottle to obtain the black tea leaf extract.
[0065] Tobacco flavor (percentage by weight): 15% β-Damascenone, 30% macrostigmatrienone, 5% 2,3,5-trimethylpyrazine, 8% ethyl vanillin, 4% palmitic acid , 9% dihydroactinolactone, 2%...
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