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Envelope calcium chloride and preparation method thereof

A technology of coating calcium chloride and calcium chloride, applied in the application, animal feed, animal feed and other directions, can solve the problems of difficulty in promotion, poor effect, immature calcium chloride coating technology, etc., to improve bioavailability rate, low application cost, and the effect of reducing blood calcium and its secondary diseases

Active Publication Date: 2015-05-06
HANGZHOU KINGTECHINA FEED CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] However, the current coating technology for calcium chloride is not yet mature, and the effect of solving the problem of moisture absorption is not good, so it is difficult to promote

Method used

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  • Envelope calcium chloride and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A kind of coated calcium chloride, the concrete steps of its preparation method are as follows:

[0029] (1) Dissolve 600g of calcium chloride in water to prepare a saturated aqueous solution of calcium chloride, take 100g of silicon dioxide and put it into a granulation fluidized bed, atomize it with saturated aqueous solution of calcium chloride as the mother liquor, and spray it into Spray granulation is carried out from inside the fluidized bed to the surface of silica. During the spray granulation process, the inlet air temperature is 62°C, the outlet air temperature is 55°C, the atomization pressure is 0.2Mpa, and the speed of the peristaltic pump is 200r / min. Obtain first-level coated particles;

[0030] (2) Add 100g hydrogenated castor oil and 100g calcium palmitate (the mass fraction of palmitic acid is 43%) into the mixer, heat and melt at 80°C, then add the first-level coated particles, and mix for 10min; put the above mixture Put into a 75kW granulator with...

Embodiment 2

[0033] A kind of coated calcium chloride, the concrete steps of its preparation method are as follows:

[0034] (1) Dissolve 750g of calcium chloride in water to prepare a saturated aqueous solution of calcium chloride, take 100g of silicon dioxide and put it into a granulation fluidized bed, atomize it with saturated aqueous solution of calcium chloride as the mother liquor, and spray it into Spray granulation is carried out from inside the fluidized bed to the surface of silica. During the spray granulation process, the inlet air temperature is 65°C, the outlet air temperature is 53°C, the atomization pressure is 0.2Mpa, and the peristaltic pump speed is 200r / min. Obtain first-level coated particles;

[0035] (2) Add 50g of hydrogenated castor oil and 50g of calcium palmitate (the mass fraction of palmitic acid is 45%) into the mixer, heat and melt at 80°C, then add the first-level coated particles, and mix for 12min; put the above mixture Put into 75kW aperture and be in t...

Embodiment 3～6 and comparative example 1～3

[0038] The coating calcium chloride preparation method of embodiment 3~6 and comparative example 1~3 is except that the parameter listed in table 1 is different with embodiment 1, all the other contents are identical with embodiment 1.

[0039] Adopt the same preparation method as Example 1, only some parameters in the preparation method are different; Comparative Example 1 and Comparative Example 2 are also basically the same as the preparation method of Example 1, only the raw material composition ratio of coated calcium chloride Different, Comparative Example 3 uses different raw material compositions, specifically as shown in Table 1, and the parts not mentioned in Table 1 are the same as in Example 1.

[0040] The coated calcium chloride obtained carries out the mensuration of dissolution rate, and detection method is:

[0041](1) Adjust the temperature of the dissolution tester to 37°C and the rotational speed to 100r / min, pour the artificially prepared simulated rumen f...

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Abstract

The invention discloses envelope calcium chloride and a preparation method thereof. The envelope calcium chloride is prepared from the following raw materials in parts by weight: 5-20 parts of hydrogenated palm oil, 5-20 parts of hydrogenated castor oil, 4-30 parts of silicon dioxide, 1-20 parts of fatty acid calcium and 60-85 parts of calcium chloride. The preparation method is characterized in that the envelope calcium chloride which can be taken as a feed additive is obtained by taking the hydrogenated palm oil, the hydrogenated castor oil, silicon dioxide and fatty acid calcium as envelope materials and taking the calcium chloride as a core material through a multiple-time pelletizing and enveloping technology. The envelope calcium chloride can make up the defects that the calcium chloride raw material easily absorbs water, and also can guarantee that calcium chloride safely passes through a rumen to smoothly reach the intestinal tract, so that the biological utilization rate of calcium chloride is greatly increased.

Description

technical field [0001] The invention relates to the technical field of feed additives, in particular to coated calcium chloride and a preparation method thereof. Background technique [0002] Calcium chloride is an inorganic compound, a salt composed of chlorine and calcium elements, and is a typical ionic halide. The molecular formula of calcium chloride is CaCl 2 , the relative molecular weight is 110.98, and the properties are white, hard fragments or granules, slightly bitter, and odorless. Calcium chloride has strong hygroscopicity and is easily deliquified when exposed to the air. It is easily soluble in water and emits a lot of heat at the same time. Its aqueous solution is slightly alkaline. [0003] Calcium chloride is often used as an anion salt additive in dairy cow diets. It has the functions of supplementing the anions required by dairy cows, reducing the DCAD (dietary ion balance) value of dairy cows, improving the acid-base balance of dairy cows’ body fluids...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23K1/00A23K1/175
Inventor 李浙烽陈强徐二华许美芳
Owner HANGZHOU KINGTECHINA FEED CO LTD
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