Preparation method of rice straw biochar
A technology of rice straw and biochar is applied in the field of preparation of rice straw biochar, which can solve the problem of low utilization rate of rice straw, and achieve the effects of improving comprehensive utilization rate and added value, mild reaction conditions and increasing economic benefits.
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[0023] Embodiments of the present invention provide a method for preparing rice straw biochar, comprising the following steps:
[0024] The rice straw is crushed, mixed with water, and then introduced into a hydrothermal reaction kettle for hydrothermal carbonization reaction. The ratio of the mass of the rice straw to the volume of water is 1kg:5L~1kg:20L; the product of the hydrothermal carbonization reaction is cooled , separated by filtration, and dried to obtain rice straw biochar.
[0025] In the above technical solution, the present invention realizes the comprehensive utilization of rice straw, increases the added value, and can fix carbon and reduce emissions, and obtains a product that can be used for environmental pollution restoration, and has better economic and social benefits.
[0026] As a preferred solution, the present invention also includes a pretreatment step of the rice straw: removing soil and sundries on the surface of the rice straw.
[0027] As a pre...
Embodiment 1
[0035] Such as figure 1 As shown, rice straw biochar was prepared according to the following steps:
[0036] Step 1. Recycling and pretreatment of rice straw: after the rice is harvested, the remaining rice straw is recycled, and the soil and sundries on the surface of the rice straw are removed;
[0037] Step 2, crushing of rice straw: crushing the rice straw to obtain small particles and small lumps of raw materials (less than 1 cm in length), storing them for later use;
[0038] Step 3. Hydrothermal carbonization of rice straw: mix rice straw with water, import it into a hydrothermal kettle, ensure that the hydrothermal kettle is airtight, and heat for hydrothermal carbonization reaction. The hydrothermal reaction temperature is 150 o C, reaction time 14 h, rice straw raw material and water-solid-liquid ratio 1kg:5L;
[0039] Step 4. Filtration and separation of solid and liquid phase products: After the hydrothermal carbonization process, stop heating, and cool the hydro...
Embodiment 2
[0042] Step 1. Recycling and pretreatment of rice straw: after the rice is harvested, the remaining rice straw is recycled, and the soil and sundries on the surface of the rice straw are removed;
[0043] Step 2, crushing of rice straw: crushing the rice straw to obtain small particles and small lumps of raw materials (less than 1 cm in length), storing them for later use;
[0044] Step 3. Hydrothermal carbonization of rice straw: mix rice straw with water, import it into a hydrothermal kettle, ensure that the hydrothermal kettle is airtight, and heat it for hydrothermal carbonization reaction. The hydrothermal reaction temperature is 200 o C, reaction time 6 h, rice straw raw material and water-solid-liquid ratio 1kg:10L;
[0045] Step 4. Filtration and separation of solid and liquid phase products: After the hydrothermal carbonization process, stop heating, and cool the hydrothermal reactor to below 80 oAfter C, open a still to export reaction solution and solid phase produ...
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