Flame retardation PTT polyester fiber and preparation method therefor
A technology of polyester fiber and flame retardant, which is applied in the field of flame-retardant PTT polyester fiber and its preparation, which can solve the problems of low dimensional stability, poor flame retardancy, and poor heat resistance, and achieve soft and excellent hand feeling. Flame retardant performance and heat resistance performance, and the effect of strong wearability
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Embodiment 1
[0018] A kind of flame-retardant PTT polyester fiber, its components are proportioned by mass percentage: PTT 85%, flame retardant monomer 8%, polyethylene glycol 4%, phenylmethyl silicone 1.5%, perfluorobutyl Potassium sulfonate 0.1%, trimethyl phosphate 0.3%, antioxidant 0.3%, pentaerythritol stearate 0.8%, wherein, the PTT is made from terephthalic acid and 1,3-propanediol Polytrimethylene terephthalate with an intrinsic viscosity of 0.7-0.9dL / g, the flame retardant monomer is 2-hydroxyethyl (phenyl) phosphinic acid, and the antioxidant is tetrakis[β-(3 , 5-di-tert-butyl-4-hydroxyphenyl) propionate] pentaerythritol ester.
[0019] Preparation method: (1) Preparation of flame retardant monomer pre-polymerization liquid: take flame retardant monomer and a certain mass of 1,3-propanediol and add it to esterification, so that 1,3-propanediol is used as solvent, flame retardant The mass percent concentration of the flame retardant monomer is 20-40wt% slurry, and then add the ca...
Embodiment 2
[0021] A kind of flame-retardant PTT polyester fiber, its components are proportioned by mass percentage: PTT 91%, flame retardant monomer 5%, polyethylene glycol 2.5%, phenylmethyl silicone 1%, perfluorobutyl Potassium sulfonate 0.1%, triphenyl phosphate 0.1%, antioxidant 0.1%, pentaerythritol stearate 0.2%, wherein, the PTT is prepared from terephthalic acid and 1,3-propanediol Polytrimethylene terephthalate with an intrinsic viscosity of 0.7-0.9dL / g, the flame retardant monomer is 2-hydroxyethyl (phenyl) phosphinic acid, and the antioxidant is tetrakis[β-(3 , 5-di-tert-butyl-4-hydroxyphenyl) propionate] pentaerythritol ester.
[0022] Preparation method: (1) Preparation of flame retardant monomer pre-polymerization liquid: take flame retardant monomer and a certain mass of 1,3-propanediol and add it to esterification, so that 1,3-propanediol is used as solvent, flame retardant The mass percent concentration of the flame retardant monomer is 20-40wt% slurry, and then add th...
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