Production method of metal deactivator
A technology of metal deactivator and production method, applied in the direction of chemical instruments and methods, catalyst protection, physical/chemical process catalysts, etc., can solve the problems of poor stability, large dosage, high toxicity, etc., and achieve the effect of optimizing the production process
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[0016] A production method of a metal deactivator, comprising the following steps: A, its main components include 400-500kg of mother liquor A, 60-200kg of mother liquor B and 7-30kg of a pH regulator, after adding deionized water, stirring for 30- 60;
[0017] B. Preparation of mother liquor A: first, add 1-30kg of pH regulator, 20-40kg of organic acid, and 30-90kg of organic amine into a 630kg reaction flask, and stir for 20min; then add 90-230kg of antimony powder, and continue to increase the temperature by 50 Add 130-200 kg of oxidizing agent dropwise at ~100°C, condense and reflux for 1-2 hours; finally add 35-40 kg of stabilizer, stir and cool down to room temperature, and discharge to obtain mother liquor A; in the step B, the pH regulator is ethylenediamine. In the step B, the organic acid is benzoic acid. In the step B, the organic amine is monoethanolamine or diethanolamine. In the step B, the stabilizer is one or more of potassium carbonate, ammonium dihydrogen p...
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