Preparation method and application of artabotrys hexapetalus essential oil microcapsule

A technology of volatile oil and eagle's claw flower, which is applied in the preparation and application field of eagle's claw flower volatile oil microcapsules, can solve the problems such as no public literature reports, and achieve the effect of simple and feasible technical route, mild conditions, and avoiding oxidation and volatilization

Inactive Publication Date: 2015-09-30
NANJING ZELANG MEDICAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] Through literature search, do not see the public literature report identical with the present invention

Method used

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  • Preparation method and application of artabotrys hexapetalus essential oil microcapsule

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Mix 0.5 parts by mass of stabilizer polydimethyldiallylammonium chloride with 66 parts by mass of chitosan (viscosity-average molecular weight of 300,000, degree of deacetylation>90%) and sodium alginate aqueous solution (mass ratio of 3:1:8) mixed, stirred and dissolved to obtain solution A; add 3 parts by mass of emulsifier monoglyceride and 30 parts by mass of volatile oil of Eagle Claw Flower to solution A, stir at 10000r / min for 10 minutes and then pass in High-pressure homogenizer, homogenize three times under the conditions of temperature 70°C and pressure 30MPa to form a mixture with uniform particle size, and obtain solution B; stir solution B at a constant temperature of 40°C, adjust the pH value to 5.5, and obtain recoagulation liquid Cool the recondensation liquid, then adjust the pH value to 7, add 0.5 parts by mass of glyoxal, react, move into a 30°C water bath to solidify, and obtain the volatile oil microcapsule emulsion of the hawk's claw flower; centrif...

Embodiment 2

[0028] Mix 1 mass part of stabilizer polyacrylamide with 74 mass parts of chitosan (viscosity average molecular weight is 500,000, deacetylation degree > 90%) and sodium alginate aqueous solution (mass ratio is 3:1:8), Stir and dissolve to obtain solution A; add 4 parts by mass of emulsifier monoglyceride and 20 parts by mass of the volatile oil of Eagle Claw Flower to solution A, stir at 15000r / min at a high speed for 10min, and then pass it into a high-pressure homogenizer, at a temperature of 75 Homogenize three times under the conditions of ℃ and pressure 40MPa to form a mixture with uniform particle size, and obtain solution B; stir solution B at a constant temperature of 45°C, adjust the pH value to 6.0, and obtain a re-coagulation liquid; cool the re-coagulation liquid, and then Adjust the pH value to 7.5, add 1 mass part of vanillin, react, transfer to a water bath at 40°C to solidify, and obtain the volatile oil microcapsule emulsion of Eagle Claw Flower; centrifuge, w...

Embodiment 3

[0030] Mix 0.5 parts by mass of stabilizer polyacrylamide with 70 parts by mass of chitosan (viscosity-average molecular weight of 400,000, degree of deacetylation>90%) and sodium alginate aqueous solution (mass ratio of 3:1:8), Stir and dissolve to obtain solution A; add 3.5 parts by mass of emulsifier monoglyceride and 25 parts by mass of the volatile oil of Eagle's Claw Flower to solution A, stir at 12000r / min at a high speed for 10min, and then pass it into a high-pressure homogenizer, at a temperature of 80 Homogenize three times under the conditions of ℃ and pressure 50MPa to form a mixture with uniform particle size, and obtain solution B; stir solution B at a constant temperature of 50°C, adjust the pH value to 6.5, and obtain a recoagulation liquid; cool the recoagulation liquid, and then Adjust the pH value to 8, add 1 mass part of vanillin, react, transfer to a 35°C water bath to solidify, and obtain the volatile oil microcapsule emulsion of the hawk's claw flower; c...

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Abstract

The invention discloses a preparation method and application of an artabotrys hexapetalus essential oil microcapsule. The preparation method comprises the following steps: dissolving chitosan, sodium alga acid and a stabilizer with water, and stirring evenly to obtain a solution A; adding an emulsifier and artabotrys hexapetalus essential oil to the solution A, and homogenizing to obtain a solution B; stirring the solution B at a constant temperature of 40-50 DEG C, and adjusting the pH value to 5.5-6.5 to obtain a compound gel; cooling the compound gel, and then adjusting the pH value to 7-8; and adding a curing agent, reacting and curing to obtain the artabotrys hexapetalus essential oil microcapsule. The obtained artabotrys hexapetalus essential oil microcapsule is in a powder form, is relatively good in water solubility and stability, high in embedding rate, and slow to release, has significant antibacterial activity, and can be applied to the fields such as daily chemicals and medicines.

Description

technical field [0001] The invention relates to a preparation method and application of hawk claw flower volatile oil microcapsules. Background technique [0002] Accordia stenosa is a plant of the genus Accordiaceae of tomato litchi. There are more than 100 species of this genus in the world, and they are mainly distributed in tropical and subtropical regions. In the folk, the stenotic eagle claw flower has been used as a medicinal plant for a long time. It has the functions of clearing away heat and detoxification, reducing inflammation and relieving pain, and can also be used to treat lymphatic tuberculosis of the head and neck. [0003] Volatile oil is a class of active ingredients in traditional Chinese medicine, widely distributed in the plant kingdom, and has a variety of pharmacological activities and a wide range of uses. It is mainly used as flavor in various foods and daily chemical products, and the functional research on volatile oil has not yet been carried ou...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/185A61K9/50A61P31/04A61K47/36
Inventor 刘东锋杨成东
Owner NANJING ZELANG MEDICAL TECH
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