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Method for preparing crocodile ossein chelated calcium

A technology for chelating calcium and collagen, which can be used in food preparation, medical preparations containing active ingredients, drug combinations, etc. Effect

Active Publication Date: 2015-10-07
孝感顺利特种养殖有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, it cannot meet the needs of the market

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039]The preparation method of crocodile bone collagen chelated calcium of the present invention, the preparation method of described collagen chelated calcium comprises the following process steps:

[0040] Step 1. Collect materials, take crocodile bones and remove the blood, flesh and connective tissue between the bones, but keep the tendons and cartilage on the bones, and then wash them with warm water at 40°C;

[0041] Step 2. Freezing. Put the above-mentioned cleaned crocodile bones into a freezer to freeze at a temperature of -30°C and a freezing time of 40 hours;

[0042] Step 3, normal temperature treatment, take out the crocodile aggregate from the freezer, and make it return to room temperature 20°C;

[0043] Step 4, cooking, the crocodile aggregates treated at normal temperature are then subjected to high temperature of 130°C and high pressure cooking of 0.169MPa for 1 hour;

[0044] Step 5, microwave treatment, take out the above-mentioned crocodile bones after c...

Embodiment 2

[0056] Example 2 is basically the same as Example 1, except that: the water temperature in the step 1 is 48°C; the freezing temperature in the step 2 is -38°C, and the freezing time is 50 hours; the room temperature in the step 3 22°C; the high temperature in the step 4 is 140°C, the high pressure is 0.286MPa, and the cooking time is 2 hours; the gap treatment in the step 5 is 25 minutes, and the low temperature is 80°C. The microwave low-temperature gap treatment refers to microwave heating for 5 After 5 minutes, stop and cool for 5 minutes, then turn on the machine and heat it for 5 minutes, then stop it for cooling for 5 minutes, then turn it on and heat it for 5 minutes, and then stop it; in the step 7, the ultrafine pulverized particles are 800 mesh; in the step 8, the pot The temperature is 36°C, pH 7.8, enzymolysis for 100 minutes; the pot temperature in step 9 is 52°C, pH 7.4, and enzymolysis for 130 minutes; the amount of distilled water added in step 12 is 1.8 times t...

Embodiment 3

[0058] Example 3 is basically the same as Example 1, except that: the water temperature in the step 1 is 50°C; the freezing temperature in the step 2 is -40°C, and the freezing time is 60 hours; the room temperature in the step 3 25°C; in step 4, the high temperature is 150°C, the high pressure is 0.375MPa, and the cooking time is 3 hours; in the step 5, the gap treatment is 30 minutes, and the low temperature is 100°C. The microwave low-temperature gap treatment refers to microwave heating for 5 After 5 minutes, stop the machine and cool it for 5 minutes, then turn it on and heat it for 5 minutes, then turn it off and cool it for 5 minutes, then turn it on and heat it for 5 minutes, then stop it and cool it for 5 minutes; in the step 7, the ultrafine pulverized particles are 900 mesh; The pot temperature in step 8 is 37°C, pH 8, enzymolysis for 2 hours; the pot temperature in step 9 is 55°C, pH 7.5, enzymolysis for 2.25 hours; the amount of distilled water added in step 12 is ...

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Abstract

The invention discloses a method for preparing crocodile ossein chelated calcium. The method includes the following process steps: (1) materials are obtained; (2) freezing is carried out; (3) normal-temperature processing is carried out; (4) stewing is carried out; (5) microwave processing is carried out; (6) smashing is carried out; (7) superfine grinding is carried out; (8) first-time enzymolysis is carried out; (9) second-time compounded enzymolysis is carried out; (10) the materials obtained after two times of enzymolysis are placed into a centrifugal machine for separation; (11) concentration and spraying drying are carried out to obtain ossein protein peptide powder; (12) separated bone powder is taken out for acidolysis for extracting calcium powder; (13) centrifugation is carried out to obtain bone calcium powder; (14) water bath chelation is carried out; and (15) powdered crocodile ossein chelated calcium is obtained. The crocodile ossein chelated calcium is high in quality and can be widely applied to the fields of medicines, foods, health care and the like.

Description

technical field [0001] The invention relates to a preparation method of a calcium supplement, in particular to a preparation method of crocodile collagen chelated calcium. Background technique [0002] Calcium is one of the most abundant elements in the human body, ranking fifth after carbon, hydrogen, oxygen, and nitrogen, accounting for about 1.5-2.0% of the total human body. It has a very important function to the life activities of the human body. It is not only the main component of building bones and teeth, but also an element that maintains the normal excitation of muscle nerves, activates various enzymes, and participates in the blood coagulation process. It maintains blood permeability, osmotic pressure, and acid-base balance, so it is an indispensable element in maintaining human metabolism and life activities, including material transformation and transmission, heart beat, and muscle movement, and must be continuously supplemented. [0003] The standard of daily...

Claims

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Application Information

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IPC IPC(8): A61K38/39C12P21/06A23L1/29A61P3/02
Inventor 郑正炯吴颖江丽张田骏
Owner 孝感顺利特种养殖有限公司
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