Ultrathin oriented silicon steel sheet and short-process manufacturing method thereof

A manufacturing method and technology of oriented silicon, applied in the field of electrical steel manufacturing, can solve the problems of many product defects, easy cracking of thin strips, high energy consumption, etc., and achieve the effect of simplifying the production process, simple manufacturing method and low energy consumption

Active Publication Date: 2015-10-07
NORTHEASTERN UNIV
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Problems solved by technology

[0003] However, the production of oriented silicon steel by the conventional secondary recrystallization method has a thickness limit of the finished product, which is generally about 0.15mm. When the thickness is lower than this thickness, the secondary recrystallization of the finished product is not perfect, or secondary recrystallization cannot occur. As a result, the magnetic properties are very poor, and the required service performance cannot be achieved; in order to obtain oriented silicon steel thin strips with a thickness of ≤0.15mm, people now use the three-time recrystallization production process as follows: First, use the traditional production process to obtain 0.20~0.35mm thick The secondary recrystallized oriented silicon steel is cold-rolled to a target thickness of 0.15mm or less after removing the glass film and insulating film on the surface of the finished plate, and then annealed at 750~1000°C to obtain an extremely thin strip of oriented silicon steel by triple recrystallization; the above The defects in the production process are: the thin strip is easy to crack and break during cold rolling, and the cold rolling efficiency is low; moreover, the current process needs to use the finished plate of oriented silicon steel as raw material, and the traditional production process of oriented silicon steel has many product defects. , low yield, high energy consumption, serious environmental pollution and other shortcomings

Method used

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  • Ultrathin oriented silicon steel sheet and short-process manufacturing method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] The molten steel composition of ultra-thin grain-oriented silicon steel sheet is C 0.04%, Si 3.0%, Mn 0.18%, S 0.022%, Als 0.025%, N 0.0095%, O8 1.80T, iron loss P 10 / 400 6.6W / kg, P 10 / 1000 22.0 W / kg, thickness 0.1mm;

[0040] The molten steel for smelting has the same composition as above;

[0041] A twin-roll strip continuous casting device is used to pour molten steel through the tundish into a cavity composed of two crystallization rollers and two side sealing plates to form a molten pool. The upper surface superheat of the molten pool is controlled at 40°C, and the molten steel in the molten pool Solidified with the rotation of the crystal roll and exported at a speed of 40m / min to obtain a cast belt;

[0042] The cast strip is cooled by the cooling unit at a speed of 60°C / s and then hot-rolled. The rolling start temperature is 1000°C, the hot-rolling reduction rate is 33.3%, the final rolling temperature is above 800°C, and the hot-rolling temperature is 60°C / s....

Embodiment 2

[0050] The molten steel composition of ultra-thin grain-oriented silicon steel sheet is C 0.002%, Si 2.8%, Mn 0.05%, S 0.015%, Als 0.005%, N 0.003%, Cu 0.3%, Sn 0.1%, O8 1.72T, iron loss P 10 / 400 is 8.1W / kg, P 10 / 1000 19.2W / kg, thickness 0.05mm;

[0051] Manufacturing method is the same as embodiment 1, and difference is:

[0052] (1) Molten steel for smelting, with the same composition as above;

[0053] (2) The superheat degree on the upper surface of the molten pool is 10°C, and the molten steel is exported at a speed of 60m / min;

[0054] (3) The cast strip is cooled at a rate of 20 °C / s, the hot rolling start temperature is 900 °C, the reduction rate is 15%, and the hot rolling is cooled at a rate of 20 °C / s;

[0055] (4) The normalization treatment temperature is 850°C, the time is 10min, and the normalization treatment cooling rate is 5°C / s;

[0056] (5) The first cold rolling reduction rate is 40%; the intermediate annealing temperature is 800°C, and the time is 10 ...

Embodiment 3

[0061] The molten steel composition of ultra-thin grain-oriented silicon steel sheet is C 0.08%, Si 3.4%, Mn 0.30%, S 0.04%, Als 0.05%, N 0.007%, Cu 0.6%, Sn 0.2%, O8 1.83T, iron loss P 10 / 400 is 7.1 W / kg, P 10 / 1000 27.2W / kg, thickness 0.15mm;

[0062] Manufacturing method is the same as embodiment 1, and difference is:

[0063] (1) Molten steel for smelting, with the same composition as above;

[0064] (2) The superheat degree on the upper surface of the molten pool is 70°C, and the molten steel is exported at a speed of 20m / min;

[0065] (3) The cast strip is cooled at a rate of 100 °C / s, the hot rolling start temperature is 1150 °C, the reduction rate is 50%, and the hot rolling is cooled at a rate of 100 °C / s;

[0066] (4) The normalization treatment temperature is 1150°C, the time is 1min, and the normalization treatment cooling rate is 50°C / s;

[0067] (5) The first cold rolling reduction rate is 70%; the intermediate annealing temperature is 1100 ° C, and the time i...

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Abstract

The invention relates to an ultrathin oriented silicon steel sheet and a short-process manufacturing method thereof. The steel sheet comprises the following components in percentage by mass: 0.002-0.08% of C, 2.8-3.4% of Si, 0.05-0.30% of Mn, 0.015-0.04% of S, 0.005-0.05% of Als, 0.003-0.010% of N, 0-0.6% of Cu, 0-0.2% of Sn, less than 0.004% of O, less than 0.01% of P and the balance of Fe. The thickness of the product is 0.05-0.15mm. The manufacturing method comprises the following steps: (1) smelting molten steel; (2) carrying out continuous casting to obtain a casting band; (3) cooling, carrying out hot rolling and coiling; (4) carrying out normalizing treatment and controlled cooling; (5) pickling, and carrying out primary cold rolling; carrying out interannealing; (6) pickling, and carrying out secondary cold rolling; carrying out decarburizing annealing; (7) coating an annealing separant; and (8) carrying out high-temperature annealing and purification annealing. The method greatly simplifies the ultrathin oriented silicon steel sheet production process, is simple and effective, and has the characteristics of short process, high controllability and low energy consumption.

Description

technical field [0001] The invention belongs to the field of electrical steel manufacturing, and in particular relates to an ultra-thin oriented silicon steel plate and a short-flow manufacturing method thereof. Background technique [0002] Grain-oriented silicon steel (including ordinary grain-oriented silicon steel and high magnetic induction grain-oriented silicon steel) is a soft magnetic material containing about 3% silicon. Due to its strong {110}<001> Gauss texture, it has a very low Iron loss and very high magnetic induction intensity, mainly used in the manufacture of transformer cores; it is the only product in the iron and steel industry that uses the secondary recrystallization phenomenon, and is a relatively successful application of texture control technology in industrial production; by reducing the orientation The iron loss of silicon steel and saving a lot of electric energy is the goal that people pursue unremittingly. Reducing the thickness of grain...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C38/16C21D8/12B22D11/06
Inventor 刘海涛王银平宋红宇刘文强张宝光赵士淇安灵子曹光明李成刚刘振宇王国栋
Owner NORTHEASTERN UNIV
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