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Novel magnetic active carbon and preparation method thereof

A magnetic activated carbon, a new type of technology, applied in chemical instruments and methods, other chemical processes, alkali metal oxides/hydroxides, etc., can solve the problems of complex preparation conditions and difficulty in mass production, and reduce processing costs. Good reuse effect, enhanced application feasibility and market competitiveness effect

Inactive Publication Date: 2015-12-09
HIT YIXING ACAD OF ENVIRONMENTAL PROTECTION +1
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Problems solved by technology

In recent years, one of the solutions is to improve the adsorption performance and magnetic separation characteristics of synthetic materials by loading magnetic nano-substances on the adsorption materials, but there are often problems such as complex preparation conditions and difficulty in mass production. In addition, how to achieve The simple and effective means of regeneration of adsorption materials is also the key point in the improvement process of adsorption materials.

Method used

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  • Novel magnetic active carbon and preparation method thereof
  • Novel magnetic active carbon and preparation method thereof
  • Novel magnetic active carbon and preparation method thereof

Examples

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Embodiment 1

[0024] Example 1: A new type of magnetic activated carbon, powdered activated carbon: PAC and nano-iron oxide: Fe 3 o 4 of composite materials. PAC / Fe 3 o 4 The mass ratio is 1.

[0025] A preparation method of a new type of magnetic activated carbon, using chemical co-precipitation method, in Fe 3+ / Fe 2+ (Molar ratio)=2 In the reaction system, powdered activated carbon is used as a carrier to complete the reaction by adding lye medium;

[0026] The Fe 3+ / Fe 2+ (molar ratio)=2 reaction system is FeCl3 / FeSO4 (molar ratio)=2 or FeCl3 / FeCl2 (molar ratio)=2;

[0027] The lye medium is NaOH;

[0028] Powdered activated carbon is PAC.

[0029] The specific steps of the chemical co-precipitation method are: 1. PAC is dried in an oven for 24 hours at a temperature of 100 ° C; The solution is mixed at a temperature of 50°C, and a certain amount of PAC is added to the mixed solution to control the PAC / Fe in the composite material. 3 o 4 ratio, and continued to stir, then ...

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Abstract

The invention discloses a novel magnetic active carbon and a preparation method thereof. The novel magnetic active carbon is a composite material of powdered active carbon (PAC) and nano iron oxide (Fe3O4). Reaction is finished by feeding an alkaline liquid medium into a reaction system Fe<3+> / Fe<2+> (mole ratio)=2 which takes the powered active carbon as a carrier by adopting a chemical co-precipitation method; the ratio of PAC to the iron oxide in the magnetic active carbon is adjusted by controlling the PAC feeding amount so as to optimize the performance of the material. The preparation method has the advantages of simple operation, quickness, batch production, high reproducibility and the like. The novel magnetic active carbon has the performances of large adsorption amount, easiness in separation, recycling and regeneration, good repeated use effect and the like; the problems that the conventional PAC is high in difficulty when separated from treated wastewater and easy to lose, and cannot be regenerated, and the treatment cost is high are well solved; regeneration can be easily and efficiently realized by feeding H2O2, so that the treatment cost of the adsorption technology is reduced, and the feasibility of application of the novel magnetic active carbon into actual engineering and the market competitiveness are improved.

Description

technical field [0001] The invention relates to the field of water treatment, in particular to magnetic activated carbon and a preparation method thereof. technical background [0002] With the maturity of activated carbon treatment technology, activated carbon technology has been widely used in many fields as a water treatment technology capable of removing various pollutants. People often use this method as a general treatment method to solve various sewage problems (such as printing and dyeing wastewater). Activated carbon can be divided into two categories according to its size: powder activated carbon (PAC) and granular activated carbon (GAC). It has the disadvantages of light specific gravity, difficulty in separating from treated water, easy loss, non-recyclable, and high treatment cost. Powdered activated carbon is almost always used once in my country, and it is usually combined with other processes (such as coagulation, activated sludge method) to enhance the trea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/20B01J20/28B01J20/30C02F1/28C02F1/58C02F101/38
Inventor 郭海娟周家晖马放
Owner HIT YIXING ACAD OF ENVIRONMENTAL PROTECTION
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