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Solvent-free single-component wet-curing polyurethane court elastic material sizing agent and preparation method

An elastic material and single-component technology, applied in the field of stadium elastic material slurry and its preparation, can solve the problems of solvent pollution and increased material cost, and achieve the effects of low slurry viscosity, cost saving, and convenient construction

Inactive Publication Date: 2015-12-09
王亚松
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This will not only cause solvent pollution in the process of product production, site construction and later use of the site, but also the solvent will evaporate in the end, which increases the cost of materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] The polyether polyol PPG220400Kg that number average molecular weight is 2000, functionality is 2, number average molecular weight is 3000, polyether polyol PPG3050100Kg that functionality is 3, plasticizer DOP240Kg, talcum powder 400Kg, ground calcium carbonate 500Kg, Put 8Kg of dispersant and 2Kg of pigment phthalocyanine green into a 2000L reaction kettle; start stirring and raise the temperature to 100°C, vacuumize and dehydrate. , heat up to 80°C and keep it warm for 2 hours; then, add 2Kg of catalyst dibutyltin dilaurate, continue to keep warm for half an hour, then add 180Kg of viscosity reducer, BYK-525Kg of defoamer, and 1010 antioxidant [four [β-( 3,5-di-tert-butyl-4-hydroxyphenyl) propionic acid] pentaerythritol ester] 5Kg, ultraviolet absorber UV-9 (2-hydroxyl-4-methylbenzophenone) 5Kg, continue to stir for half an hour; Sampling and testing, packaging after passing the test.

Embodiment 2

[0037] The polyether polyol PPG210150Kg that number average molecular weight is 1000, functionality is 2, number average molecular weight is 4800, polyether polyol PPG330350Kg that functionality is 3, plasticizer TXIB200Kg, talcum powder 400Kg, ground calcium carbonate 400Kg, Put 5Kg of dispersant and 2Kg of pigment phthalocyanine green into a 2000L reactor; start stirring and heat up to 100°C, vacuumize and dehydrate, and stop the vacuum after the moisture content reaches below 0.05% by weight; cool down to 60°C, add MDI-50130Kg , heat up to 80°C and keep it warm for 2 hours; then, add 4Kg of catalyst bismorpholine diethyl ether, continue to keep warm for half an hour, then add 160Kg of viscosity reducer, latent curing agent (2-isopropyl-3-hydroxyethyl -1,3-oxazolidine) 10Kg, defoamer BYK-524Kg, antioxidant 1076 [β-(3,5-di-tert-butyl-4-hydroxyphenyl) octadecyl propionate] 5Kg , UV absorber UV-9 (2-hydroxy-4-methylbenzophenone) 5Kg, continue to stir for half an hour; sampling ...

Embodiment 3

[0039] Put polyether polyol PPG330800Kg with a number average molecular weight of 3000 and a functionality of 3, plasticizer DOTP200Kg, talc powder 300Kg, heavy calcium carbonate 400Kg, dispersant 5Kg, pigment phthalocyanine green 2Kg into a 2000L reactor; start stirring And raise the temperature to 100°C, vacuumize and dehydrate. After the moisture content reaches below 0.05% by weight, stop the vacuum; cool down to 60°C, add MDI-50125Kg, raise the temperature to 80°C and keep it warm for 2 hours; then, add the catalyst dilauric acid Dibutyltin 2Kg, continue to keep warm for half an hour, then add viscosity reducer 150Kg, defoamer BYK-523Kg, antioxidant 1010 [tetrakis [β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionic acid ] Pentaerythritol ester] 5Kg, ultraviolet absorber UV-9 (2-hydroxy-4-methylbenzophenone) 5Kg, continue to stir for half an hour; sampling test, packaging after passing the test.

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PUM

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Abstract

The invention relates to a solvent-free single-component wet-curing polyurethane court elastic material sizing agent and preparation method. The sizing agent is prepared by adopting the following raw material formula: 25 to 40 parts of polyurethane pre-polymer with an end sealed by NCO, 20 to 45 parts of inorganic packing, 10 to 15 parts of plasticizer, 8 to 12 parts of viscosity reducer and 10 to 25 parts of functional additive; the polyurethane pre-polymer with the end sealed by the NCO is a reaction product of polyether glycol and excessive diisocyanate. According to the sizing agent prepared by adopting the formula and a process provided by the invention, the weakness that an existing material needs to be diluted by adding an organic solvent so as to be used can be solved; the sizing agent contains no organic solvent, thereby being small in viscosity, good in self leveling performance and convenient for construction; meanwhile, the solvent pollution during the material production, field construction and field application processes can be avoided, and the environmental friendliness can be realized; moreover, no organic solvent is contained, thus fewer material is used for per unit construction area of the same thickness, and the cost is saved.

Description

technical field [0001] The invention relates to a court elastic material slurry and a preparation method thereof, in particular to a solvent-free one-component moisture-cured polyurethane court elastic material slurry and a preparation method thereof. Background technique [0002] In recent years, with the rise of the sports industry, the sports field laying industry has developed rapidly. Polyurethane materials have also been greatly developed as excellent sports ground paving materials. The use of traditional two-component polyurethane paving materials requires on-site measurement and mixing, which is laborious and prone to errors, and requires high requirements for construction workers. [0003] In 2005, Jiangmen Changhe Group launched a silane-modified one-component polyurethane flooring material and named it Silicon PU. The material has good cushioning and ductility, strong adhesion, has a certain healing function on the foundation, can be automatically leveled, simpl...

Claims

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Application Information

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IPC IPC(8): C08L75/08C08L91/06C08K3/26C08K3/34C08K5/12C08K5/103C08G18/48
Inventor 刘永磊王亚松
Owner 王亚松
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