Antibacterial masterbatches used for plastic toys and preparation method of antibacterial masterbatches
A technology for antibacterial masterbatch and plastic toys, applied in the field of antibacterial masterbatch of plastic toys and its preparation, can solve the problems of agglomeration, uneven dispersion, and the inability of antibacterial agents to have antibacterial, anti-aging and health care functions at the same time.
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Embodiment 1
[0028] 1. Preparation of raw materials:
[0029] ①Preparation of loess powder: collect a certain amount of loess and send it into a muffle furnace, calcinate at 450°C for 1.5h, and pulverize it into a 90-mesh fine powder after cooling. Stir and react at 75°C for 2 hours, then add an appropriate amount of 30wt% NaOH solution to adjust the pH value to neutral, stir and react at room temperature for 1.5 hours, filter, wash the filter cake with deionized water for 3 times, and blow dry at 100 , ground to a particle size of 1000 mesh to obtain white loess powder;
[0030] ②Preparation of Bellflower, Geranium, and Agrimony extracts: Collect the non-decomposed Bellflower, Geranium, and Agrimony, wash them separately, dry them, cut them into 0.5cm pieces, and pour them into the corresponding In the extraction tank, add ethanol with a concentration of 75wt% according to 9 times the weight of the fragments. After soaking for 3 hours, reflux extraction for 1.5 hours, filter, and extract...
Embodiment 2
[0039] 1. Preparation of raw materials:
[0040] ①Preparation of loess powder: collect a certain amount of loess and put it into a muffle furnace, calcined at 350°C for 3 hours, and after cooling, crush it into 80-mesh fine powder. Stir and react at 65°C for 3 hours, then add an appropriate amount of 30wt% NaOH solution to adjust the pH value to neutral, stir and react at room temperature for 1.5 hours, filter, wash the filter cake twice with deionized water, and dry it with air at 100°C. Grind to a particle size of 900 mesh to obtain white loess powder;
[0041]②Preparation of bellflower, geranium, and agrimony extracts: collect bellflower, geranium, and agrimony without decay, wash them separately, dry them, cut them into 1.2cm pieces, and pour them into the corresponding In the extraction tank, add ethanol with a concentration of 85wt% according to 7 times the weight of the fragments, soak for 2 hours, reflux for extraction for 1 hour, filter, and extract the filter residu...
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