Sweetener composition, method for manufacturing same and use thereof

A manufacturing method and a technology for a composition, applied in the field of body, can solve the problems of difficulty in refining, significant coloring of the product, disproportionate industrial production efficiency, etc., and achieve excellent effects in terms of sweetness and physical properties.

Inactive Publication Date: 2015-12-16
MATSUTANI CHEM INDS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If this reaction is utilized, the sugar can be isomerized, so a small amount of rare sugar can be obtained (Non-Patent Document 5), but to obtain the isomerized product containing the rare sugar at the concentration showing the above-mentioned physiological activity, there is a need to work with The actual industrial production efficiency is not commensurate with the reaction time, the color of the product due to side reactions such as caramelization is remarkable, and the subsequent purification is difficult, etc., and it is difficult to use industrially.

Method used

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  • Sweetener composition, method for manufacturing same and use thereof
  • Sweetener composition, method for manufacturing same and use thereof
  • Sweetener composition, method for manufacturing same and use thereof

Examples

Experimental program
Comparison scheme
Effect test

experiment example A

[0139]

[0140] Using sugar and hydrochloric acid, a 0.7 mol / l hydrochloric acid solution containing 3% (w / v) of sugar was prepared. This was hydrolyzed at a temperature of 40° C. for 20 minutes, 30 minutes, 50 minutes, and 80 minutes, respectively. After neutralizing the decomposed solution with sodium hydroxide, it was analyzed by HPLC (detector: RI, column: Mitsubishi Chemical Corporation MCIGELCK08EC, mobile phase: water, flow rate: 0.4ml / min) (this analysis condition is also used in the following experimental examples) same.).

[0141] The sugar composition (%) of the obtained hydrolyzate is shown in Table 1 below.

[0142] [Table 1]

[0143]

[0144] Next, in order to confirm whether the sugar composition obtained by acid hydrolysis is similarly decomposed at different concentrations, the sugar composition under acid hydrolysis conditions at 90°C was confirmed for a 80% (w / w) solution of granulated sugar, and it was confirmed that break down.

[0145] In addition,...

experiment example B～D

[0146]

[0147] Using sugar and invertase (manufactured by MPBiomeicals, Inc., 100 unit / mg), a 3% (w / v) sugar solution containing invertase (0.003% w / w, sugar g) was prepared. This was hydrolyzed at a temperature of 40° C. for 20 minutes, 30 minutes, and 40 minutes, respectively, and HPLC analysis was performed in the same manner as in Example 1.

[0148] The sugar composition (%) of the obtained hydrolyzate is shown in Table 2 below.

[0149] [Table 2]

[0150]

[0151] Next, a 25% (w / v) sucrose solution containing invertase (0.00075% w / w, saccharose g) was prepared and subjected to 10 minutes, 20 minutes, 30 minutes, 40 minutes, and 50 minutes at a temperature of 40°C. , 60 minutes, 70 minutes, and 80 minutes of hydrolysis, HPLC analysis was performed in the same manner.

[0152] The sugar composition (%) of the obtained hydrolyzate is shown in Table 3 below.

[0153] [table 3]

[0154]

[0155] Further, commercially available invertase (manufactured by DSM, 200 ...

experiment example E

[0161]

[0162] Each solution of the enzymatic hydrolyzate obtained in the experimental areas C3, C4, and C5 in Experimental Example 2 was prepared to 0.1M NaOH, and the isomerization reaction was performed at a temperature of 60° C. for 2 hours. A part of the reaction liquid after the isomerization reaction was sampled, and the sugar composition was analyzed by HPLC.

[0163] The sugar composition of the obtained alkali isomerization reaction product is shown in Table 5 below.

[0164] [table 5]

[0165]

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Abstract

The present invention provides a novel sweetener, which is free from a risk of diseases caused by the intake of isomerized sugars and overcomes problems encountered in the course of producing a rare sugar-containing syrup or disadvantages in taste, a method for manufacturing the same, and a use thereof. A method for manufacturing a sweetener composition, said method comprising: treating sucrose with an acid and / or an enzyme under specific conditions to thereby efficiently decompose sucrose into glucose and fructose; and then isomerizing the obtained mixture using an alkali and / or an enzyme under specific conditions in such a manner as to allow the resultant isomerized product to contain D-psicose mainly as a rare sugar so that the product comprises, at a specific composition ratio, sucrose, D-glucose, D-fructose and rare sugar(s) at least containing D-psicose, or the product comprises, at a specific composition ratio, D-glucose, D-fructose and rare sugar(s) at least containing D-psicose.

Description

technical field [0001] The present invention relates to a method for producing a desired sweetener composition using sugar as a raw material, the produced sweetener composition, and its use. Alternatively, a method for a sweetener composition containing D-psicose in a mixed sugar mainly composed of glucose and fructose, the obtained sweetener composition, and uses thereof. Background technique [0002] Isomerized sugar produced by saccharifying starch into a saccharification solution and treating it with glucose isomerase is widely used in beverages and foods including soft drinks because it has the same sweetness as granulated sugar and is inexpensive to produce. Used as a sweetener, the world's production of isomerized sugar reaches 17.3 million tons (statistics in 2009). A typical production method of this isomerized sugar is to hydrolyze starch with enzymes to produce amylolysis product (dextrin), then further hydrolyze it with other enzymes to produce a glucose solutio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/22A23L1/30A61K8/60A61K31/7004A61P3/04A61P3/06A61Q19/06A23L23/00A23L27/00A23L27/60
CPCA61K8/60A61K31/7004A61Q19/06A23L27/33A23L33/20A61P3/04A61P3/06C13K1/02C13K3/00C13K11/00C13K13/00A61K2300/00
Inventor 新谷知也吉川谅P·K·古洛帕利何森健
Owner MATSUTANI CHEM INDS CO LTD
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