Preparation method of nano-material with bismuth oxybromide loaded on cobalt nickel hydrotalcite surface
A surface loading, bismuth oxybromide technology, applied in chemical instruments and methods, water pollutants, other chemical processes, etc., to achieve the effect of simple and easy operation of the experimental process, good prospects for development, and high catalytic repeatability
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[0025] Cobalt-nickel hydrotalcite surface loaded bismuth oxybromide (BiOBr / Co-Ni-NO 3 LDHs) The preparation method of nano-photocatalytic materials includes the following steps:
[0026] (1) At room temperature, add cobalt chloride, nickel chloride and hexamethylene tetramine with a molar ratio of 2:1:18 to ultrapure water in sequence, fully dissolve them, and put them into a hydrothermal reactor. React at ℃ for 5h, after cooling, the product is separated by filtration, and washed with deionized water and ethanol, and finally dried at room temperature to obtain cobalt nickel hydroxide;
[0027] (2) At room temperature, weigh 0.372g of cobalt-nickel hydroxide into an eggplant-shaped bottle containing 200mL of acetonitrile and 13.34mmol of bromine water. First add bromine water and blow in nitrogen for 15 minutes, then wrap the bottle tightly. Do not leak air, and keep stirring for 24 hours, then centrifuge the product, clean it with a large amount of ethanol, and finally dry it at r...
Example Embodiment
[0031] Example 1
[0032] At room temperature, weigh 0.9517 g of cobalt chloride hexahydrate, 0.4754 g of nickel chloride hexahydrate, and 5.0468 g of hexamethylenetetramine into 400 mL of ultrapure water, and stir until completely dissolved. Divide it into 5 equal parts into a 100mL hydrothermal reactor, and react in an oven at 95°C for 5 hours. After cooling, the product was filtered and washed with deionized water and ethanol 3 times each, and dried at room temperature to obtain Co-Ni hydroxide.
Example Embodiment
[0033] Example 2
[0034] At room temperature, measure 0.69 mL of bromine water and dissolve it in an eggplant-shaped bottle, add 200 mL of acetonitrile and 0.372 g of Co-Ni hydroxide samples in sequence, and wrap the mouth of the bottle with plastic wrap. Then access N 2 15min, and continue to stir for 24h. The product was centrifuged and washed with a large amount of ethanol, and dried at room temperature to obtain Co-Ni-BrLDH.
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