Green production technology for bromothalonil
A technology for green production and bromoxynil, applied in the field of green production technology of bromoxynil, can solve problems such as pollution and unfriendly environment, and achieve the effects of reducing production cost, high product yield and good crystal form
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[0026] The following examples are used to illustrate the present invention, but should not be used to limit the scope of the present invention. The implementation conditions used in the examples can be further adjusted according to the manufacturer's conditions, and the unspecified implementation conditions are usually conventional experimental conditions.
[0027] The specific embodiment of the green production technology of a kind of bromothalonil of the present invention is described in detail as follows:
[0028] A kind of green production technique of bromothalonil, comprises the steps:
[0029] 1) Get 120kg of triethylamine, and vacuum the liquid into the high-level metering tank for subsequent use;
[0030] 2) Use the same pumping method to pump 1350kg of acrylonitrile into the 2000L reactor, control the temperature of the material to about 30°C, add 80kg of crushed zinc chloride from the manhole and start stirring for 60 minutes, the zinc chloride will be completely d...
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