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Preparation method of carbon fiber reinforced titanium alloy composite material

A technology of composite materials and titanium alloys, which is applied in the field of preparation of carbon fiber reinforced titanium alloy composite materials, can solve the problems of reduced tensile and shear resistance of carbon fibers, poor chemical compatibility and physical compatibility, and low bonding force of composite materials And other problems, to achieve high tensile and shear resistance, improve chemical compatibility and physical compatibility, and good product quality

Inactive Publication Date: 2016-01-13
迈克瑞(珠海)复合材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to combine the carbon fiber into the metal block by mechanical compounding or directly metallurgical, because the carbon fiber has a smooth surface, high inertness, and few chemically active functional groups, so it is chemically compatible with the titanium alloy matrix. Poor physical and chemical compatibility, carbon fiber is difficult to compound into titanium alloy, resulting in low bonding force of the composite material, easy to detach during use, and the disadvantages of reduced tensile and shear resistance of carbon fiber. A carbon fiber reinforced titanium alloy is provided. The preparation method of the alloy composite material, the polyacrylamide of the present invention is used as a raw material to prepare carbon fibers, soaked with organic matter after spinning, then spinning and mixing with the obtained titanium dioxide suspension, loading titanium dioxide on the spinning, and then mixing with metal titanium , obtained after oven drying and calcination

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0021]First, take 2kg of Spirogyra and 2kg of ramie stems and wash them with clean water once respectively, air dry them naturally, and then sterilize them under ultraviolet light for 1 hour to remove stains and impurities, put the Spirogyra and ramie stems in a closed container, and add deionized water Soak for 10 minutes. After the soaking is completed, add 20% water and 10% cellulase to hydrolyze for 30 minutes to obtain a mixed enzymatic hydrolysis solution; Add 1% yeast and 3% water to the fermentation broth, and seal and ferment at 25°C for 8 days. After the fermentation is completed, add ethyl acetate solution with a mass fraction of 18% and a mass fraction of 98% acetic acid solution, control the temperature at 28°C, set the speed at 500r / min, stir magnetically for 30min, let it stand for 1h, and filter the precipitate; take 4g of polyacrylamide particles and put them into the Erlenmeyer flask, and add 50mL of water to it, control The temperature is 25°C, and the tempe...

example 2

[0023] First, take 2.5kg of spirogyra and 2.5kg of ramie stems and wash them twice with clean water, air-dry them naturally, and then sterilize them under ultraviolet light for 2 hours to remove stains and impurities. Ionized water was soaked for 15 minutes. After the soaking was completed, 25% water and 12% cellulase were added for enzymolysis for 40 minutes to obtain a mixed enzymolysis solution; Add 1.5% yeast and 4% water to the fermenter, seal and ferment at 28°C for 10 days. After the fermentation is completed, add ethyl acetate solution with a mass fraction of 20% and a mass fraction of 98% acetic acid solution, control the temperature at 32°C, set the speed at 600r / min, stir magnetically for 35min, let it stand for 1.5h, and filter the precipitate; put 6g of polyacrylamide particles into the Erlenmeyer flask, and add 55mL of Water, control the temperature at 30°C, then heat up to 105°C with programmed stirring at a speed of 5°C / min, keep the temperature and stir for 25...

example 3

[0025] First, take 3kg of spirogyra and 3kg of ramie stems and wash them twice with clean water, air-dry them naturally, then sterilize them under ultraviolet light for 3 hours to remove stains and impurities, put the spirogyra and ramie stems in an airtight container, and add deionized water Soak for 20 minutes. After soaking, add 30% water and 15% cellulase to hydrolyze for 50 minutes to obtain a mixed enzymatic solution; Add 2% yeast and 5% water to the fermentation broth, and ferment in a sealed container at 30°C for 12 days. After the fermentation is completed, add ethyl acetate solution with a mass fraction of 23% and a mass fraction of 98% to the fermentation broth. acetic acid solution, control the temperature at 35°C, set the speed at 700r / min, stir magnetically for 40min, let it stand for 2h, and filter the precipitate; take 8g of polyacrylamide particles and put them into the conical flask, and add 60mL of water to it, control The temperature is 35°C, then the tempe...

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Abstract

The invention discloses a preparation method of a carbon fiber reinforced titanium alloy composite material, and belongs to the field of preparation of composite materials. The cleaning, the disinfection, the sterilization and the enzymolysis are performed for spirogyra and ramie stems; the spirogyra and the ramie stems are put in a fermentation tank for fermenting, and are mixed with ethyl acetate and acetic acid for standing; polyacrylamide is added for mixing and extruding to obtain a cake-shaped carbon fiber material; the cake-shaped carbon fiber material is added in extraction liquid, prepared cotton leaves and chlorophytum comosum, for leaching after the yarn extraction, and is spun for mixing with prepared titanium dioxide turbid liquid; and titanium dioxide is loaded on spun yarns, is mixed with metal titanium, is dried by an oven, and is calcined to obtain the carbon fiber reinforced titanium alloy composite material. The preparation method has the following beneficial effects: the method is simple in preparation process; as carbon fibers are treated, the chemical compatibility and the physical compatibility between the carbon fibers and titanium alloy matrixes are improved; and the obtained product is excellent in quality, is high in bonding force, is not easy to be extracted in use, and is high in material stretching resistance and shearing resistance.

Description

technical field [0001] The invention relates to a method for preparing a carbon fiber reinforced titanium alloy composite material, belonging to the field of composite material preparation. Background technique [0002] Titanium is an important structural metal developed in the 1950s. Titanium alloys are widely used in various fields because of their high strength, good corrosion resistance, and high heat resistance. Many countries in the world have recognized the importance of titanium alloy materials, researched and developed them one after another, and obtained practical applications. In the 1950s and 1960s, it mainly developed high-temperature titanium alloys for aero-engines and structural titanium alloys for airframes. In the 1970s, a batch of corrosion-resistant titanium alloys were developed. Since the 1980s, corrosion-resistant titanium alloys and high-strength titanium alloys have been further developed. develop. Titanium alloys are mainly used to make aircraft e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C47/04C22C49/11C22C101/10C22C121/02
Inventor 梅庆波盛艳花
Owner 迈克瑞(珠海)复合材料有限公司
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