Macromolecule heat conduction and dissipation blended composite material and automatic preparation method

A composite material and polymer technology, which is applied in the fields of polymer thermal conduction and heat dissipation blended composite materials and automatic preparation, can solve the problems of ineffective improvement of thermal conductivity, influence of continuity of production, uneven dispersion of thermally conductive fillers, etc., and saves energy. The effect of manpower, uniform dispersion and promotion, shortening production cycle

Inactive Publication Date: 2016-01-27
东莞市万江明冠实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the first method, due to the high filling amount of thermally conductive powder, it is very easy to cause difficulty in cutting the material during extrusion and granulation, which seriously affects the continuity of production, and easily causes the thermally conductive filler to disperse in the matrix resin Uneven, unable to form an effective heat conduction network, so that the heat conduction performance of the material cannot be effectively improved
In the second method, taking into account the defects of the first method, the heat-conducting powder is mixed wi...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0027] An automatic preparation method for polymer thermal conduction and heat-conducting blended composite materials, comprising the steps of:

[0028] 1) First use powder surface activation treatment agent to surface-treat the thermally conductive filler in a high-speed mixer for 20 minutes;

[0029] 2) Then enter another high-speed mixer through an automatic conveying device, and mix with other raw materials evenly;

[0030] 3) Automatically convey the mixture obtained in the previous step to the internal mixer for internal mixing and kneading for 15 minutes;

[0031] 4) The obtained mixture can be directly extruded into a twin-screw extruder for granulation.

Embodiment 1

[0034]First, add 40 parts of alumina and 5 parts of aluminum nitride into the high-speed mixer, then add 0.6 parts of silane coupling agent KH-550, and perform surface treatment on the heat-conducting powder for 20 minutes by high-speed stirring, and the obtained pretreated powder Send in the internal mixer that 53.1 parts of PBT resins, 0.4 parts of antioxidant 1010, 0.4 parts of antioxidant 168, 0.5 parts of TAF lubricant and 5 parts of SBS-g-MAH toughening agent are housed through automatic conveying device, in Internal mixing and kneading were carried out at 240° C. for 15 minutes, and then the obtained mixture was automatically conveyed to a twin-screw extruder for extrusion and granulation.

[0035] The raw materials in this example are all calculated in parts by mass, and the total mass parts of the feed is 100 parts, the same below.

Embodiment 2

[0037] First, add 40 parts of alumina, 6 parts of aluminum nitride and 2.5 parts of boron nitride into the high-speed mixer, then add 0.7 parts of silane coupling agent KH-550, and conduct surface treatment on the heat-conducting powder for 20 minutes by high-speed stirring , the obtained pretreatment powder is sent to the container with 40.2 parts of PA6 resin, 0.4 part of antioxidant 1010, 0.6 part of antioxidant 168, 0.2 part of PETS lubricant, 0.4 part of PE wax and 9 parts of EPDM-g through the automatic conveying device - In the internal mixer of MAH toughening agent, perform internal mixing and kneading at 220° C. for 15 minutes, and then automatically transfer the obtained mixture to a twin-screw extruder for extrusion and granulation.

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Abstract

The invention discloses a macromolecule heat conduction and dissipation blended composite material. The macromolecule heat conduction and dissipation blended composite material is prepared from, by mass, 35-75 parts of matrix resin, 0-10 parts of flexibilizer, 20-50 parts of heat conduction filler, 0.2-1.0 part of antioxidant 1010, 0.2-1.0 part of phosphite ester antioxidant 168, 0.5-1.5 parts of powder surface activation treating agents and 0.5-1.5 parts of lubricant. An automatic preparation method of the macromolecule heat conduction and dissipation blended composite material includes the steps of firstly, conducting surface treating on heat conduction filler for 20 min through powder surface activation treating agents in a high-speed stirring machine; secondly, making the heat conduction filler enter another high-speed stirring machine through an automatic conveying device to be evenly mixed with other materials; thirdly, automatically conveying the mixture obtained in the second step to an internal mixer to be mixed and kneaded for 15 min; fourthly, making the obtained mixture directly enter a double-screw extruder to be extruded and granulated. The prepared heat conduction and dissipation material has the high mechanical property and heat conduction performance, automatic and continuous production is achieved, a large amount of labor is saved, the production period is greatly shortened, the production cost is greatly reduced, and the macromolecule heat conduction and dissipation blended composite material can be widely applied to the fields of LED illumination, electronic electrical appliances, automobiles and the like where good heat conduction and dissipation performance is required.

Description

technical field [0001] The invention relates to a high-molecular conduction and heat-dissipating blended composite material and an automatic preparation method. Background technique [0002] In recent years, due to a series of excellent properties such as lower density than metals and ceramics, high degree of freedom in product design, and easy processing and molding, polymer thermally conductive composite materials have become increasingly widely used in LED lighting, electronic heat sinks and other fields. This kind of material is mainly made by blending heat-conducting powder such as alumina with a polymer resin matrix, and using the heat-conducting powder to form a heat-conducting network in the polymer resin matrix to achieve the effect of heat dissipation. Its preparation method mainly has two kinds of one-step method and two-step method: one is to mix the heat-conducting powder with resin raw materials and other components, and then directly extrude and granulate thro...

Claims

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Application Information

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IPC IPC(8): C08L67/02C08L77/02C08L67/04C08L55/02C08L25/06C08L81/02C08L69/00C08L23/12C08K13/06C08K9/06C08K3/22C08K3/28C08K3/38C08K3/08C08K3/04C08K7/06
Inventor 孔作万陈明发
Owner 东莞市万江明冠实业有限公司
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