Alkaline leavening agent microcapsule and preparation method thereof
A technology of microcapsules and leavening agents, which is applied in the directions of food ingredients as leavening agents, gas-containing food ingredients, and oil-containing food ingredients, etc. To avoid problems such as the dosage of the agent, the preparation conditions are easy to control, the preparation process is simple, and the granulation is good.
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[0013] Second aspect, the present invention provides the preparation method of the alkaline leavening agent microcapsule described in the first aspect, it comprises the following steps:
[0014] (1) The core material powder and glyceryl monostearate are placed in an autoclave, and high-pressure CO is added to the autoclave. 2 , heated to form a supercritical state and fully stirred to form a suspension;
[0015] (2) Slowly release the pressure during stirring until the pressure in the reactor drops to normal pressure to obtain a white granular final product.
[0016] Preferably, in the step (1), the temperature is raised to a pressure in the autoclave of 8-30 MPa.
[0017] Preferably, the depressurization rate in the step (2) is 1-5 L / min.
Embodiment 1
[0020] Weigh 1g of sodium bicarbonate and pulverize it until it passes through a 80 mesh sieve; weigh 20g of glyceryl monostearate, place the core material and wall material in an autoclave; CO 2 , the temperature is raised to form a supercritical state, the pressure in the autoclave reaches 8Mpa, and it is fully stirred to form a suspension; then the CO is released at a speed of 1L / min during stirring. 2 , the pressure in the reactor drops to normal pressure, and during the depressurization process, the CO 2 When the supercritical fluid state is lost, the wall material glyceryl monostearate dissolved therein gradually precipitates out and covers the surface of the core material to obtain white granular matter, which is sodium bicarbonate microcapsules.
Embodiment 2
[0022] Weigh 1g of ammonium bicarbonate and pulverize it until it passes through a 80 mesh sieve; weigh 15g of glyceryl monostearate, place the core material and wall material in an autoclave; CO 2 , heated up to form a supercritical state, the pressure in the autoclave reached 12MPa, and was fully stirred to form a suspension; then CO was released at a rate of 2L / min during stirring. 2 , the pressure in the reactor drops to normal pressure, and during the depressurization process, the CO 2 When the supercritical fluid state is lost, the wall material glyceryl monostearate dissolved therein gradually precipitates out and covers the surface of the core material to obtain white granules, which are ammonium bicarbonate microcapsules.
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