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A kind of zinc oxide ink for printing electronics and its preparation method and use method

A technology of zinc oxide and electronics, applied in the direction of ink, application, household utensils, etc., to achieve the effect of strong stability, low curing temperature and good adhesion

Active Publication Date: 2018-12-21
NORTHEASTERN UNIV LIAONING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Functional material inks for printing electronics are mainly divided into two types: particle type and particle-free type. Among them, the particle type ink is composed of metal oxide particles, dispersants, surfactants, solvents and other additives, which need to be sintered at a higher temperature, which limits its application on flexible substrates such as PET

Method used

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  • A kind of zinc oxide ink for printing electronics and its preparation method and use method
  • A kind of zinc oxide ink for printing electronics and its preparation method and use method

Examples

Experimental program
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Effect test

Embodiment 1

[0028] The composition of the zinc oxide ink for printed electronics in this embodiment is, by mass percentage, zinc acetate:ammonia water:ethanol=10%:25%:65%.

[0029] The preparation method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0030] According to the formula of zinc oxide ink for printed electronics, first dissolve ammonia water in ethanol, mix for 10 minutes to achieve uniformity, then add zinc acetate to the mixture, stir for 3 hours at 25°C until dissolved, use 0.22μm micropores Zinc oxide ink for printed electronics is obtained after filtration by the filter membrane.

[0031] The usage method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0032] Zinc oxide ink for printed electronics was spin-coated on a glass substrate, heated with a heating plate in the air, and kept at 250°C for 10 minutes to obtain a zinc oxide film.

[0033] The viscosity of the zin...

Embodiment 2

[0035] The composition of the zinc oxide ink for printed electronics in this embodiment is, by mass percentage, zinc acetate: ethylenediamine: isopropanol = 45%: 30%: 25%.

[0036] The preparation method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0037] According to the formula of zinc oxide ink for printed electronics, first dissolve ethylenediamine in isopropanol, mix for 8 minutes to achieve uniformity, then add zinc acetate to the mixture, stir at 25°C for 0.5h until dissolved, use Zinc oxide ink for printed electronics is obtained after filtration through a 0.22 μm microporous membrane.

[0038] The usage method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0039] Coat the zinc oxide ink for printed electronics on the quartz substrate with a doctor blade, heat it in the air with a muffle furnace, and keep it at 330°C for 30 minutes to obtain a zinc oxide film. ...

Embodiment 3

[0042] The composition of the zinc oxide ink for printed electronics in this embodiment is, by mass percentage, zinc butyrate: isopropylamine: methanol: ethylene glycol = 40%: 37%: 15%: 7%.

[0043]The preparation method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0044] According to the formula of zinc oxide ink for printed electronics, first dissolve isopropylamine in the mixed solution of methanol and ethylene glycol, mix for 10 minutes to achieve uniformity, then add zinc butyrate to the mixed solution, and stir at 25°C for 8 hours to Dissolve and filter through a 0.22 μm microporous membrane to obtain zinc oxide ink for printed electronics.

[0045] The usage method of the printed electronic zinc oxide ink of the present embodiment comprises the following steps:

[0046] Coating the zinc oxide ink wire bar for printed electronics on the glass substrate, heating in the air with a muffle furnace, and keeping the tempe...

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Abstract

The invention provides zinc oxide ink for printed electronics and a preparation method and use method of the zinc oxide ink. The ink is prepared from, by mass, 10-50% of a chelating agent, 25-66% of a complexing agent and 8-65% of solvent; the preparation method of the zinc oxide ink for printed electronics includes the steps that the chelating agent or the complexing agent is dissolved in the solvent and evenly mixed, then the zinc precursor is added to the mixed liquid and stirred to be dissolved, and the zinc oxide ink for printed electronics can be obtained after filtering; the use method includes the steps that the ink is arranged on a base plate in a printed or coated mode, curing is conducted in air, and a zinc oxide film is obtained. The ink is high in stability, the preparation method is simple, easy to operate, the ink is low in cost and free of pollution, multiple printing or coating methods can be adopted, and the zinc oxide ink for printed electronics and the preparation method and use method of the zinc oxide ink have wide application in preparation of zinc oxide lines or films on a flexible substrate, glass and quartz and optoelectronic devices, such as, transparent conducting thin films, flat displays, solar cell transparent electrodes, pressure sensitive elements and gas sensitive elements.

Description

technical field [0001] The invention belongs to the field of ceramic functional inks for printing electronics, in particular to a zinc oxide ink for printing electronics and its preparation method and use method. Background technique [0002] Zinc oxide has a hexagonal wurtzite crystal structure and is a wide-bandgap semiconductor material with a direct bandgap. The bandgap width at room temperature is 3.3eV, and the exciton binding energy is as high as 60meV. ZnO thin film has good transparent conductivity, piezoelectricity, photoelectricity, gas sensitivity, pressure sensitivity and other properties, and is easy to integrate with various semiconductor materials. Therefore, it has broad application prospects in the field of optoelectronic devices such as flat-panel displays, transparent electrodes of solar cells, pressure-sensitive components, and gas-sensitive components. The properties of ZnO materials involve many research fields, including: transparent conductive film ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D11/03C09D11/033C09D11/38
CPCC09D11/03C09D11/033C09D11/38
Inventor 李晓东董越孙旭东吴金蓉贾莎莎
Owner NORTHEASTERN UNIV LIAONING
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