Novel silk softening agent and preparation method thereof

A technology of softener and silk, which is applied in the field of new silk softener and its preparation, can solve the problems that cannot meet the actual production of the factory, silk is soft, fluffy, elastic, etc. The effect of low preparation cost

Inactive Publication Date: 2016-03-30
张莘蔓
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The technical problem to be solved by the present invention is to provide a new type of silk softener and its preparation method, to solve the problems that the silk is soft, fluffy, elastic, etc., and cannot meet the actual production needs of the factory after using the silk softener at present.

Method used

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  • Novel silk softening agent and preparation method thereof
  • Novel silk softening agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A new type of silk softener, in parts by weight, comprising the following raw materials: 6 parts of ester group quaternary ammonium salt, 0.3 part of silane-modified polyurethane, 0.2 part of polyether-modified silane, 0.1 part of sodium lignosulfonate, alkyl 0.1 part of sodium benzenesulfonate, 0.2 part of starch grafted sodium acrylate, 0.2 part of sodium polyacrylate, 0.2 part of sodium N-lauroyl glutamate, 0.2 part of calcium lignosulfonate, 0.2 part of citronellal, 0.3 part of malic acid , 0.1 part of carrageenan, 0.1 part of locust bean gum, 0.1 part of triadimefon, 40 parts of deionized water.

[0026] The preparation method of described novel silk softening agent comprises the following steps:

[0027] S1: Add the ester quaternary ammonium salt into deionized water, raise the temperature to 50°C, stir to dissolve the ester quaternary ammonium salt, and obtain the mixed solution A;

[0028] S2: Add starch-grafted sodium acrylate, sodium polyacrylate, sodium N-la...

Embodiment 2

[0032] A new type of silk softener, in parts by weight, comprising the following raw materials: 10 parts of ester quaternary ammonium salt, 0.5 part of silane-modified polyurethane, 0.4 part of polyether-modified silane, 0.4 part of sodium lignosulfonate, alkyl 0.3 parts of sodium benzenesulfonate, 0.4 parts of starch grafted sodium acrylate, 0.3 parts of sodium polyacrylate, 0.4 parts of sodium N-lauroyl glutamate, 0.3 parts of calcium lignosulfonate, 0.5 parts of citronellal, 0.5 parts of malic acid , 0.3 parts of carrageenan, 0.2 parts of locust bean gum, 0.3 parts of triadimefon, 70 parts of deionized water.

[0033] The preparation method of described novel silk softening agent comprises the following steps:

[0034] S1: Add the ester quaternary ammonium salt into deionized water, raise the temperature to 60°C, stir and dissolve the ester quaternary ammonium salt to obtain a mixed solution A;

[0035] S2: Add starch-grafted sodium acrylate, sodium polyacrylate, sodium N-...

Embodiment 3

[0039] A new type of silk softener, in parts by weight, comprising the following raw materials: 9 parts of ester quaternary ammonium salt, 0.4 part of silane-modified polyurethane, 0.3 part of polyether-modified silane, 0.3 part of sodium lignosulfonate, alkyl 0.2 parts of sodium benzenesulfonate, 0.3 parts of starch grafted sodium acrylate, 0.3 parts of sodium polyacrylate, 0.3 parts of sodium N-lauroyl glutamate, 0.3 parts of calcium lignosulfonate, 0.4 parts of citronellal, 0.4 parts of malic acid , 0.2 parts of carrageenan, 0.2 parts of locust bean gum, 0.3 parts of triadimefon, 60 parts of deionized water.

[0040] The preparation method of described novel silk softening agent comprises the following steps:

[0041] S1: Add the ester quaternary ammonium salt into deionized water, raise the temperature to 55°C, stir and dissolve the ester quaternary ammonium salt, and obtain the mixed solution A;

[0042] S2: Add starch-grafted sodium acrylate, sodium polyacrylate, sodium...

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Abstract

The invention discloses a novel silk softening agent and a preparation method thereof, and belongs to the technical field of softening agent processing. The novel silk softening agent comprises the follow raw materials: ester group quaternary ammonium salt, silane modified polyurethane, polyether modified silane, sodium lignosulfonate, sodium alkyl benzene sulfonate, starch grafted sodium acrylate, sodium polyacrylate, sodium N-lauroyl glutamate, calcium lignin sulfonate, citronellal, malic acid, carrageenan, locust bean gum, triadimefon, and deionized water. The novel silk softening agent is prepared by steps of ester group quaternary ammonium salt dissolution, microwave reactions, antifoaming, and pH value adjustment. The provided novel silk has a strong biodegradable performance, and is green and environment-friendly. The preparation method is simple, convenient, and feasible. The preparation cost is low, and thus the popularization and application are easy to promote.

Description

technical field [0001] The invention belongs to the technical field of softener processing, and in particular relates to a novel silk softener and a preparation method thereof. Background technique [0002] The process of processing silk quilts in the traditional way is simple, and the variety is extremely single. After the silk quilts processed by the traditional process are used, the silk fibers are easy to tangle and stick, and the elasticity and warmth will be reduced accordingly, requiring frequent dismantling and tearing Loose, in order to maintain the original excellent clothing performance of silk quilt. [0003] In order to endow silk with excellent properties such as bulkiness, softness, and high elasticity, it is necessary to refine the silk to expand the voids of the silk fibers, and the resulting silk cotton has the characteristics of bulkiness, high elasticity, and no knots between fibers. Through the puffing treatment of silk, the bulkiness, high elasticity a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/46D06M15/564D06M15/53D06M15/01D06M15/263D06M13/342D06M13/165D06M15/03D06M13/352D06M101/10
CPCD06M13/46D06M13/165D06M13/342D06M13/352D06M15/01D06M15/03D06M15/263D06M15/53D06M15/564D06M2101/10D06M2200/50
Inventor 张莘蔓
Owner 张莘蔓
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