Two-layer-method two-sided flexible copper clad plate
A flexible copper-clad laminate, double-sided technology, applied in the field of two-layer double-sided flexible copper-clad laminates, can solve the problems of TPI performance, high process requirements, complex process, etc., and achieve excellent copper foil bonding Good quality and compressibility, high product qualification rate, and the effect of simplifying the production process
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preparation example Construction
[0038] A two-layer double-sided flexible copper clad laminate, comprising two upper and lower copper foil layers and a polyimide insulating layer sandwiched between the two copper foil layers; its preparation method includes the following steps:
[0039] (1) synthesizing a thermosetting polyamic acid resin glue and a thermoplastic polyamic acid resin glue, and carrying out chemical imidization of the thermoplastic polyamic acid resin glue to obtain a soluble thermoplastic polyimide powder;
[0040] (2) Dissolving the soluble thermoplastic polyimide powder in a polar solvent to obtain a thermoplastic polyimide glue, mixing the thermoplastic polyimide glue with the thermosetting polyamic acid resin glue to obtain Thermosetting polyamic acid-thermoplastic polyimide mixture;
[0041] (3) Provide copper foil, coat the thermosetting polyamic acid-thermoplastic polyimide mixture on one of the surfaces of the copper foil, and then dry the coating to obtain thermosetting polyamic acid-...
Synthetic example 1
[0051] Add 360g of NMP (N-methylpyrrolidone) and DMAc (N,N-dimethylacetamide) into a 1L three-necked flask, weigh 6.50g of ODA and 16.006g of PDA, dissolve in the above polar solvent NMP and The solution was obtained in DMAc, and then the solution was cooled in a water bath, and 52.665 g of BPDA (biphenyltetracarboxylic dianhydride) was added under a nitrogen flow, the reaction temperature was controlled at 15-20 ° C, and the stirring was continued for 8 hours, and the reaction was prepared. The thermosetting polyamic acid resin glue has a solid content of 15%.
[0052] 2. Preparation of soluble thermoplastic polyimide glue
Synthetic example 2
[0054] First, prepare thermoplastic polyamic acid resin glue: add polar solvent NMP (N-methylpyrrolidone) and DMAc (N,N-dimethylacetamide) to a 1L three-necked flask, 460g in total, and weigh 8.654g of BAPS And the BAPP of 32.841g, it is dissolved in the above-mentioned polar solvent NMP and DMAc to obtain solution, this solution is cooled in water bath, adds the BPDA of 11.697g and the ODPA of 18.631g under nitrogen stream (3,3 ', 4, 4'-diphenyl ether dianhydride), the reaction temperature is controlled to be 15-20° C., and the stirring is continued for 8 hours, and the reaction is carried out to prepare a thermoplastic polyamic acid resin glue solution, wherein the solid content is 14%;
[0055] Subsequent imidization: take 40ml of acetic anhydride and 20ml of pyridine, mix them, add them to the thermoplastic polyamic acid resin glue prepared above, stir and react at room temperature for 24 hours, pour the mixture into a sufficient amount of deionized water to obtain a thermo...
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