Preparation method of adhesive coating, wear resistant and flame resistant floor leather for vehicle
A technology for floor leather and vehicles, applied in the field of floor leather preparation, can solve problems such as unpleasant smell, surface wear and tear, and affect air quality, and achieve a remarkable effect of wear resistance
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example 1
[0024]Add 10g of antimony chloride and 0.3g of polyethylene glycol to 200mL of absolute ethanol, ultrasonically disperse for 10min until completely dissolved, then transfer to a 500mL three-neck flask equipped with a stirrer and dropping funnel, and drop 10mL of 0.5mol / L ammonium fluoride solution, and adjust the pH to 8 with ammonia water with a mass concentration of 5%, to obtain a mixed solution; transfer the above mixed solution into a water bath, heat up to 30°C, and start the agitator to stir at a constant temperature for complexation reaction After 2 hours, pour the reactant into a Buchner funnel, filter with suction to obtain a filter residue, put the filter residue in a vacuum drying oven at 80° C. to dry to constant weight, and then grind to obtain a white nanometer antimony trioxide powder; weigh 5 g of the above-prepared Disperse nanometer antimony trioxide powder into 50mL deionized water, add 2g aliphatic amine polyoxyethylene ether, stir evenly with a glass rod, ...
example 2
[0030] Add 11g of antimony chloride and 0.4g of polyethylene glycol to 250mL of absolute ethanol, ultrasonically disperse for 15min until completely dissolved, then transfer to a 500mL three-necked flask with a stirrer and dropping funnel, and drop 11mL of 0.5mol / L ammonium fluoride solution, and adjust the pH to 9 with ammonia water with a mass concentration of 5%, to obtain a mixed solution; transfer the above mixed solution into a water bath, heat up to 35°C, and start the stirrer to stir at a constant temperature for complexation reaction After 2 hours, the reactant was poured into a Buchner funnel, and the filter residue was obtained by suction filtration. The filter residue was put into a vacuum drying oven at 83° C. to dry to constant weight and then ground to obtain white nano antimony trioxide powder; weigh 8 g of the above-prepared Disperse nano antimony trioxide powder into 80mL deionized water, add 2g aliphatic amine polyoxyethylene ether, stir evenly with a glass r...
example 3
[0036] Add 12g of antimony chloride and 0.5g of polyethylene glycol to 300mL of absolute ethanol, ultrasonically disperse for 20min until completely dissolved, then transfer to a 500mL three-necked flask with a stirrer and dropping funnel, and drop 12mL of 0.5mol / L ammonium fluoride solution, and adjust the pH to 10 with ammonia water with a mass concentration of 5%, to obtain a mixed solution; transfer the above mixed solution into a water bath, heat up to 40°C, and start the stirrer to stir at a constant temperature for complexation reaction After 3 hours, the reactant was poured into a Buchner funnel, and the filter residue was obtained by suction filtration. The filter residue was put into a vacuum drying oven and dried to constant weight at 85° C., and then ground to obtain white nanometer antimony trioxide powder; weigh 10 g of the above-prepared Disperse nano antimony trioxide powder into 100mL deionized water, add 3g aliphatic amine polyoxyethylene ether, stir evenly wi...
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