Self-repair powder coating applicable to aluminum material
A powder coating and self-healing technology, applied in the field of coatings, can solve problems such as appearance deformation of powder materials
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Embodiment 1
[0009] Epoxy resin: 500 parts; precipitated barium sulfate: 400 parts; 40 parts of curing agent, 5 parts of charge regulator, 25 parts of pigment; mixed and extruded by twin-screw extruder. After secondary crushing, 30 parts of self-repairing microcapsules and 6 parts of catalyst were added and mixed evenly. Preparation of self-healing microcapsules: Dissolve urea in 2.5% ethylene maleic anhydride EMA solution under stirring environment, after the urea is completely dissolved, add appropriate amount of ammonium chloride and resorcinol; adjust the reaction with hydrochloric acid and sodium hydroxide System pH = 4.5, then add dicyclopentadiene, after the stable emulsion is formed, finally add 37% formaldehyde solution, the ratio of urea and 37% formaldehyde solution is 1:2; the above reaction system is heated to React at 55°C for 5 hours; cool to room temperature, filter and wash, and air-dry; sieve to get the product of 200-220 mesh.
Embodiment 2
[0011] Epoxy resin: 500 parts; precipitated barium sulfate: 380 parts; 40 parts of curing agent, 5 parts of charge regulator, 25 parts of pigment; mixed and extruded by twin-screw extruder. After secondary pulverization, add 50 parts of self-healing microcapsules and 10 parts of catalyst and mix well. Preparation of repair microcapsules: Dissolve urea in 2.5% ethylene maleic anhydride EMA solution under stirring environment, after the urea is completely dissolved, add appropriate amount of ammonium chloride and resorcinol; adjust the reaction system with hydrochloric acid and sodium hydroxide pH = 4.5, then add dicyclopentadiene, after the stable emulsion is formed, finally add 37% formaldehyde solution, the ratio of urea and 37% formaldehyde solution is 1:2; the above reaction system is heated to 55 React at ℃ for 5 hours; cool to room temperature, filter and wash, and air-dry; sieve to get the product of 200-220 mesh.
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