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Method for making spleen tonification preparation

A preparation method and preparation technology are applied in the field of preparation of spleen strengthening preparations, which can solve the problems of unsatisfactory clinical efficacy of spleen strengthening preparations, difficult detection of hesperidin and the like, and achieve the effects of significant medicinal effect, improved medicinal effect and high content.

Inactive Publication Date: 2016-05-25
GUIZHOU BAIHUA PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the inventor found in the course of research that the active ingredient hesperidin in tangerine peel is difficult to detect in the spleen-invigorating preparation made by the existing extraction process, which makes the clinical efficacy of the spleen-invigorating preparation not satisfactory enough.

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  • Method for making spleen tonification preparation
  • Method for making spleen tonification preparation
  • Method for making spleen tonification preparation

Examples

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Effect test

Embodiment 1

[0074] Recipe: Codonopsis 200g, fried citrus aurantium 200g, tangerine peel 200g, fried malt 200g, fried Atractylodes macrocephala 200g, fried hawthorn 150g and accessories.

[0075] Process: take tangerine peel, extract volatile oil by steam distillation, and set aside; add 10 times the amount of water to the dregs to extract twice, each time for 2 hours, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60% to the filter residue The ethanol solution was refluxed for 3 times, 1 hour each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the alcohol extract, which was combined with the above water extract, and when concentrated to 50-60°C, the relative density was 1.10-1.20 extract, get tangerine peel extract, and set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, filter, combine the filtrate, concentrate under reduced pressure t...

Embodiment 2

[0079] Recipe: Codonopsis 200g, fried citrus aurantium 200g, tangerine peel 200g, fried malt 200g, fried Atractylodes macrocephala 200g, fried hawthorn 150g and accessories.

[0080] Process: take tangerine peel, extract volatile oil by steam distillation, and set aside; add 10 times the amount of water to the dregs to extract twice, each time for 2 hours, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60% to the filter residue The ethanol solution was refluxed for 3 times, 1 hour each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the alcohol extract, which was combined with the above water extract, and when concentrated to 50-60°C, the relative density was 1.10-1.20 extract, get tangerine peel extract, and set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, filter, combine the filtrate, concentrate under reduced pressure t...

Embodiment 3

[0084] Recipe: Codonopsis 200g, fried citrus aurantium 200g, tangerine peel 200g, fried malt 200g, fried Atractylodes macrocephala 200g, fried hawthorn 150g and accessories.

[0085] Process: take tangerine peel, extract volatile oil by steam distillation, and set aside; add 10 times the amount of water to the dregs to extract twice, each time for 2 hours, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60% to the filter residue The ethanol solution was refluxed for 3 times, 1 hour each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the alcohol extract, which was combined with the above water extract, and when concentrated to 50-60°C, the relative density was 1.10-1.20 extract, get tangerine peel extract, and set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, filter, combine the filtrate, concentrate under reduced pressure t...

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Abstract

The invention discloses a method for making a spleen tonification preparation. The spleen tonification preparation is mainly prepared from codonopsis pilosula, fried immature bitter orange, dried tangerine peel, fried malt and fried hawthorn. According to the method, the specific making process and parameters of the spleen tonification preparation are improved based on properties of each drug in composition of the spleen tonification preparation and functions of the drugs in the composition, so that hesperidin, as the effective ingredient in the dried tangerine peel, is easily measured, and the content of the measured hesperidin is high; accordingly, the preparation is more refined, the efficacy is more outstanding, and the clinical efficacy is good.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine, and in particular relates to a preparation method of a spleen invigorating preparation. Background technique [0002] Extraction of traditional Chinese medicine is a commonly used method in traditional Chinese medicine pharmacy. The chemical composition of traditional Chinese medicine is extremely complex, and it is necessary to extract the active ingredients of traditional Chinese medicine that are effective for the human body from the complex mixture. to improve efficacy. [0003] The spleen-invigorating preparation is mainly made of Codonopsis pilosula, fried citrus aurantium, tangerine peel, fried malt and fried hawthorn; it has the effect of strengthening the spleen and appetizing, and is used for weak spleen and stomach, abdominal fullness, lack of food and loose stools. [0004] In the prior art, spleen-invigorating preparations are made in the following way: take fried malt an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/8998A61P1/14
CPCA61K36/344A61K9/1652A61K9/2059A61K36/284A61K36/734A61K36/752A61K36/8998A61K2236/331A61K2236/333A61K2236/39A61K2236/51A61K2236/55
Inventor 黄文荣马静
Owner GUIZHOU BAIHUA PHARMA
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